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Experimental Fourier Transform Ion Cyclotron Resonance Mass Spectrometry

  • Chapter
Experimental Mass Spectrometry

Part of the book series: Topics in Mass Spectrometry ((STMS,volume 1))

Abstract

The field of ion cyclotron resonance (ICR) mass spectrometry was established in 1949 with the invention of the omegatron mass spectrometer by Hippie et al. (1, 2) This new type of mass spectrometer employed it combination of static electric and magnetic fields to trap ions that were mass selected by applying radio frequency (rf) excitation at their cyclotron frequency and then detected on striking a collector electrode. Unfortunately, the many intriguing features of this spectrometer were countered by its poor mass resolution and mass range, and it was to find limited analytical utility. In the 1960s, ICR was investigated as a detector for studying gasphase reactive and nonreactive collisions. Wobschall constructed an ICR spectrometer that differed from the omegatron in that ionization and detection occured in separate regions of the vacuum chamber and an rf bridge circuit was used to measure ICR power absorption.(3) This instrument matured into the multisection drift ICR spectrometere(4) that combined double resonance techniques(5) with marginal oscillator detection.(6) Drift cell ICR found great utility in ion/molecule studies in the laboratories of Baldeschweiler et al.,(7) Beauchamp,(8) and Bowers et al.,(9) among others, although the technique continued to exhibit the unattractive lowperformance features of its ICR predecessors.

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Authors and Affiliations

  1. Departments of Chemistry and Biochemistry, The University of Texas at Austin, Austin, Texas, 78712, USA

    David A. Laude Jr. & Steven C. Beu

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  1. David A. Laude Jr.
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  2. Steven C. Beu
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  1. Department of Chemistry, Texas A&M University, College Station, Texas, USA

    David H. Russell

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Laude, D.A., Beu, S.C. (1994). Experimental Fourier Transform Ion Cyclotron Resonance Mass Spectrometry. In: Russell, D.H. (eds) Experimental Mass Spectrometry. Topics in Mass Spectrometry, vol 1. Springer, Boston, MA. https://doi.org/10.1007/978-1-4899-2569-5_5

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