A Note on: Development of 2-Dimensional Detectors for Radio-Thin-Layer Chromatography

  • G. Dietzel
  • H. Kubisiak
  • H. Stelzer
Chapter

Summary

The development of a series of detectors for planar radiochromatography is described (sensitivities are quoted as dpm of carbon-14). The RITA is a position sensitive proportional counter with a resolution of 0.5mm and a sensitivity of a few tens of dpm. This detector may be used, with suitable software, to analyze two dimensional thin-layer chromatography (TLC) plates. TRACY is a multiwire proportional detector which has been developed especially for two dimensional planar chromatography. This detector has a resolution of 1mm with a sensitivity of about 25dpm for an analysis time of 15 minutes. BERTA is a spark chamber which also has been developed for two dimenional radio-detection. The spark chamber has a resolution of 1mm with a sensitivity of about 10dpm in 40 minutes. One of the major disadvantages of such spark chambers has been the lack of any digital information. This has been solved by development of EVA, an optical reading system for the BERTA where a special diode array matrix is used in conjunction with a very fast Motorola 68000 CPU.

Keywords

Helium Stein Tritium IAEA Neon 

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References

  1. 1.
    P. E. Schulze and M. Wenzel, Angew.Chem.Int.Edn., 1:580 (1962).CrossRefGoogle Scholar
  2. 2.
    F. Berthold, Proceedings of Symposium on Radioisotope Sample Measurement Techniques In Medicine and Biology, IAEA, Vienna, 303 (1965).Google Scholar
  3. 3.
    G. Charpak, Proceedings of International Symposium on Nuclear Electronics, Versailles (1968).Google Scholar
  4. 4.
    A. Gabriel and S. Bram, FEBS Lett., 39: 307 (1974).PubMedCrossRefGoogle Scholar
  5. 5.
    S. Bram, French Patent FR 2279114 19.03.76 Priority date: 25.04.74 74 FR-014453.Google Scholar
  6. 6.
    C. J. Borkowski and M. K. Kopp, Rev.Sci.Instrum., 39:1515 (1968).CrossRefGoogle Scholar
  7. 7.
    C. J. Borkowski and M. K. Kopp, IEEE Trans.Nucl.Sci., 17:340 (1970).CrossRefGoogle Scholar
  8. 8.
    E. R. Flynn, S. Orbesen, N. Stein, H. Thiessen, D. M. Lee, and S. E. Sabottka, Nuclear Instruments and Methods, 111:67 (1973).CrossRefGoogle Scholar
  9. 9.
    J. Fisher, H. Okuno, and A. H. Walenta, Nuclear Instruments and Methods, 151:451 (1978).CrossRefGoogle Scholar
  10. 10.
    G. Peterson, G. Charpak, G. Melchart, and F. Sauli, Nuclear Instruments and Methods, 176:239 (1980).CrossRefGoogle Scholar
  11. 11.
    V. Perez-Mendez, Proceedings of International Meeting on Proportional and Drift Chambers, Dubna USSR, (1975).Google Scholar
  12. 12.
    B. R. Pullan, R. Howard, and B. J. Perry, Nucleonics 72, (1966).Google Scholar
  13. 13.
    B. R. Pullan and J. J. P. De Lima, Nuclear Instruments and Methods, 124:149 (1975).CrossRefGoogle Scholar
  14. 14.
    T. R. Roberts, Radiochromatography (J.Chromatogr library, 41), Elsevier/North Holland Biomedical Press, New York and Amsterdam (1978)Google Scholar

Copyright information

© Springer Science+Business Media New York 1988

Authors and Affiliations

  • G. Dietzel
    • 1
  • H. Kubisiak
    • 1
  • H. Stelzer
    • 1
  1. 1.RaytestStraubenhardt 1W. Germany

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