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5-Methylfurfuryl Alcohol

  • A. L. Mndzhoian

Abstract

A solution of 8.4 g (about 0.22 mole) of lithium aluminum hydride in 480 ml of ether (Note 1) was introduced into a 750-ml three-necked round-bottomed flask fitted with mercury-sealed stirrer, dropping funnel, and reflux condenser protected by a calcium chloride tube. The stirrer was started, and a solution of 28 g (0.2 mole) of methyl 5-methyl–2-furoate (see Vol. 1 of this work, p. 23), b.p. 97–98°/12 mm, in 150 ml of dry ether was added dropwise at such a rate that the ether boiled steadily.

Keywords

Acrylic Acid Anhydrous Sodium Sulfate Malonic Acid Reflux Condenser Dilute Hydrochloric Acid 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Literature Cited

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    D. Dinelli and G. B. Marini-Bettolo, Gazz. Chim. Ital. 71, 117 (1941) [C.A. 36, 19286 (1942)].Google Scholar
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    A. L. Mndzhoian, V. G. Afrikian, M. T. Grigorian, and E. A. Markarian, Doklady Akad. Nauk Arm. SSR (Proc. Acad. Sci. Armenian SSR) 25, 277 (1957).Google Scholar

Copyright information

© Springer Science+Business Media New York 1959

Authors and Affiliations

  • A. L. Mndzhoian

There are no affiliations available

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