2-Furyl Methyl Ketone

  • A. L. Mndzhoian

Abstract

A mixture of 34 g (0.5 mole) of furan (see Vol. 1 of this work, p. 40), b.p. 31–34°/745 mm, and 51 g (0.5 mole) of freshly distilled acetic anhydride was prepared in a 500-ml four-necked round-bottomed flask fitted with mercury-sealed stirrer, reflux condenser protected by a calcium chloride tube, thermometer, and dropping funnel. The stirrer was started, the mixture was heated to 35°, and a mixture of 5 g of 85% phosphoric acid and 50 g of 95% acetic anhydride (Note 1) was added from the dropping funnel at such a rate that the temperature of the mixture did not rise above 40°.

Keywords

Zinc Methane Ethyl Acetone Mercury 

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Copyright information

© Springer Science+Business Media New York 1959

Authors and Affiliations

  • A. L. Mndzhoian

There are no affiliations available

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