Abstract
A mixture of 56 g (0.5 mole) of 2-furoic acid (see p. 43), m.p. 128–132°, and 100 ml of dry benzene was prepared in a 300-ml round-bottomed flask fitted with reflux condenser protected by a calcium chloride tube; a solution of 71.5 g (0.6 mole) of freshly distilled thionyl chloride in 50 ml of benzene was then added. The upper end of the calcium chloride tube was connected to a Tishchenko vessel containing a solution of caustic alkali, which served to absorb hydrogen chloride and sulfur dioxide liberated during the reaction.
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Literature Cited
Lies-Bodart, C.r. 43, 393 (1856);
A. 100, 327 (1856).
P. F. Frankland and F. W. Aston, J. Chem. Soc. 79, 516 (1901)
G. Chavanne, C.r. 134, 1439 (1902).
Canadian Pat. 373,516 (1938);
C. A. 32, 50034 (1938).
E. Baum, Ber. 37, 2951 (1904);
N. N. Maxim, Bull. Soc. Chim. Romania 12, 33 (1930);
C. A. 25, 5139 (1931)
W. W. Hartman and J. B. Dickey, Ind. Eng. Chem. 24, 151 (1932).
A. L. Mndzhoian, Zh. obshchei khim. (J. Gen. Chem.) 16, 751 (1946).
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Mndzhoian, A.L. (1959). 2-Furoyl Chloride. In: Mndzhoian, A.L. (eds) Syntheses of Heterocyclic Compounds. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-6658-5_26
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DOI: https://doi.org/10.1007/978-1-4757-6658-5_26
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