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Methyl 5-Methyl-2-Furoate

  • A. L. Mndzhoian

Abstract

A mixture of 87.2 g (0.5 mole) of methyl 5-(chloromethyl)-2-furoate (see p. 29), b.p. 114–116° /3 mm, and 300 ml of 90% acetic acid was prepared in a one-liter three-necked round-bottomed flask fitted with mercury-sealed stirrer and reflux condenser. The mixture was stirred while 98 g (1.5 g-atoms) of zinc dust was added in small portions over a period of 2–2.5 hours, and with continued stirring the mixture was then boiled for 20 hours (Note 1).

Keywords

Heterocyclic Compound Anhydrous Sodium Sulfate Free Acid Sodium Carbonate Carbonate Solution 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Literature Cited

  1. 1.
    I. J. Rinkes, Rec. tray. chim. 49, 1118 (1930);Google Scholar
  2. C. A. 25, 950 (1931).Google Scholar
  3. 2.
    A. L. Mndzhoian, V. G. Afrikian, and M. T. Grigorian, Doklady Akad. Nauk Arm. SSR (Proc. Acad. Sci. Armenian SSR) 17, 166 (1953).Google Scholar
  4. 3.
    R. Andrisano, Ann. chim. (Rome) 40, 30 (1950); C. A. 45, 7563a (1951).Google Scholar

Copyright information

© Springer Science+Business Media New York 1959

Authors and Affiliations

  • A. L. Mndzhoian

There are no affiliations available

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