Advertisement

Basic SCTA Techniques

  • J. Rouquerol
  • O. Toft Sorensen
  • P. Barnes
  • E. L. Charsley
  • E. Fesenko
  • M. Reading
Part of the Hot Topics in Thermal Analysis and Calorimetry book series (HTTC, volume 3)

Abstract

Our aim, in this chapter, is to introduce the reader to the principle of operation, measurement and, sometimes also, data processing concerning the basic SCTA techniques used until now. For the sake of clarity, we shall follow the same order as in our listing of SCTA techniques in Chapter 2, i.e. based, as much as possible, both on logic and chronology. The headings of the paragraphs will use the simplest names suggested by the framework of Chapter 2, but the titles initially used by each author will also be reminded. We hope that, in this way, both logic and history will be satisfied.

Keywords

Residual Pressure Control Rate Thermal Analysis Pirani Gauge Constant Rate Thermal Analysis Isothermal Plateau 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    C.S. Smith, Trans. A.I.M.E. (Metal Division) 137 (1940) 23.Google Scholar
  2. 2.
    B. Boinon, Thesis, Université Claude Bernard, Lyon, 10th June 1974, No. d’ordre 257.Google Scholar
  3. 3.
    M. Reading, in “Thermal Analysis, Techniques and Applications” E.L. Charsley and S.B. Warrington (Eds.), Royal Society of Chemistry, Cambridge (1992) 126.Google Scholar
  4. 4.
    J. Rouquerol, Bull. Soc. Chim. Fr. (1964) 31.Google Scholar
  5. 5.
    J. Rouquerol, Thesis, Faculty of Sciences of Paris University, 19 November 1964 (Série A, No. 4348, No. d’ordre 5199).Google Scholar
  6. 6.
    F. Rouquerol, J. Rouquerol and K.S.W. Sing, “Adsorption by powders and porous solids: principles, methodology and applications”, Academic Press, London, New-York (1999) 467 p.Google Scholar
  7. 7.
    J. Rouquerol, Thermochimica Acta 300 (1997) 247.CrossRefGoogle Scholar
  8. 8.
    J. Rouquerol, J. Thermal Analysis 2 (1970) 123.CrossRefGoogle Scholar
  9. 9.
    J. Mayet, J. Rouquerol, J. Fraissard and B. Imelik, Bull. Soc. Chim. France 9 (1966) 2805.Google Scholar
  10. 10.
    P. Duran, J.L.G. Fierro, and M. Rodriguez, Meas. Sci. Technol. (1990) 523.Google Scholar
  11. 11.
    J. Rouquerol, J. Thermal Analysis, 5 (1973) 203.CrossRefGoogle Scholar
  12. 12.
    M. Ganteaume and J. Rouquerol, J. Therm. Anal. 3 (1971) 413.CrossRefGoogle Scholar
  13. 13.
    J. Rouquerol, in “Thermal Analysis”, D. Schwenker (Ed.), Academic Press, Vol. 1 (1969) 281.Google Scholar
  14. 14.
    M.H. Stacey in “Proceedings 2nd European Symposium on Thermal Analysis” (Aberdeen), D. Dollimore (Ed.), Heyden, London (1981) 408.Google Scholar
  15. 15.
    M.H. Stacey, Anal. Proc. 22 (1985) 242.Google Scholar
  16. 16.
    M. Reading and J. Rouquerol, Thermochimica Acta 85 (1985) 299.CrossRefGoogle Scholar
  17. 17.
    J. Arellano, J.M. Criado and C. Real, Thermochimica Acta 134 (1988) 365.CrossRefGoogle Scholar
  18. 18.
    C. Real, M.D. Alcala and J.M. Criado, J. Thermal Analysis 38 (1992) 797.CrossRefGoogle Scholar
  19. 19.
    P.A. Barnes, G.M.B. Parkes, D.R. Brown and E.L. Charsley, Thermochimica Acta, 269/270 (1995) 665.CrossRefGoogle Scholar
  20. 20.
    J. Rouquerol and J.M. Fulconis, ICTAC 11 Book of Abstracts, P. Gallagher (Ed.), Philadelphia (1996) 272.Google Scholar
  21. 21.
    J. Paulik and F. Paulik, Anal. Chim. Acta 56 (1971) 328.CrossRefGoogle Scholar
  22. 22.
    L. Erdey, F. Paulik and J. Paulik, Hungarian Patent No. 152197, registered 31 October 1962, published 1 December 1965.Google Scholar
  23. 23.
    J. Paulik and F. Paulik in “Comprehensive Analytical Chemistry”, G. Svehla (Ed.), Vol. XII, “Thermal Analysis”, Part A, “Simultaneous Thermo-analytical Examinations by Means of the Derivatograph”, Elsevier, Amsterdam (1981) 277 p.Google Scholar
  24. 24.
    F. Paulik, “Special Trends in Thermal Analysis”, John Wiley and Sons, Chichester (1995) 459 p.Google Scholar
  25. 25.
    H. Palmour and D.R. Johnson, in “Sintering and Related Phenomena”, G.C. Kuczynski, N.A. Hooton and C.F. Gibbon (Eds.), Gordon and Breach, New-York (1967) 779.Google Scholar
  26. 26.
    J. Paulik and F. Paulik, Proc. 5th Int. Conf. Thermal Analysis (Kyoto), Heyden, London, 1 (1977) 75.Google Scholar
  27. 27.
    F. Rouquerol and J. Rouquerol in “Thermal Analysis”, H.G. Widemann, (Ed.), Vol. 1, Birkhäuser, Basel Vol. 1, (1972) 373.Google Scholar
  28. 28.
    S. Bordère, F. Rouquerol, J. Rouquerol, J. Estienne and A. Floreancig, J. Thermal Analysis, 36 (1990) 1651.CrossRefGoogle Scholar
  29. 29.
    J. Rouquerol, Pure and Applied Chemistry 57 (1985) 69.CrossRefGoogle Scholar
  30. 30.
    G. Thevand, F. Rouquerol, and J. Rouquerol in “Thermal Analysis”, B. Miller, (Ed.), John Wiley and Sons, New-York Vol. 2 (1982) 1524.Google Scholar
  31. 31.
    M.J. Tiernan, P.A. Barnesan G.M.B. Parkes, J. Phys. Chemistry B, Vol. 103 No. 33 (1999) 6944.CrossRefGoogle Scholar
  32. 32.
    J. Rouquerol, S. Bordère and F. Rouquerol, Thermochimica Acta, 203 (1992) 193.CrossRefGoogle Scholar
  33. 33.
    A. Ortega, L.A. Pérez-Maquéda and J.M. Criado, J. Thermal Anal. 42 (1994) 551.CrossRefGoogle Scholar
  34. 34.
    R.L. Blaine, Proceedings of NATAS Meeting, R.J. Morgan (Ed.) (1997) 485.Google Scholar
  35. 35.
    R.L. Blaine, American Laboratory, January 1998, 21.Google Scholar
  36. 36.
    S.R. Sauerbrunn, B.S. Crowe and M. Reading, Proc. 21st North American Thermal Analysis Conference (1992) 137.Google Scholar
  37. 37.
    O.T. Sorensen, J. Thermal Anal. 13 (1978) 429.CrossRefGoogle Scholar
  38. 38.
    G.M.B. Parkes, P.A. Barnes, E.L. Charsley, Anal. Chem., 71 (1999) 2482–2487.CrossRefGoogle Scholar
  39. 39.
    O.T. Sorensen, J. Thermal Anal. 38 (1992) 213.CrossRefGoogle Scholar
  40. 40.
    J.C. Cloudy and J.M. Commerceron, Letoffe, Thermochim. Acta, 128 (1988) 251.CrossRefGoogle Scholar
  41. 41.
    Kraftmakher, Zh. Prikl. Mekh. & Tekh. Fiz., 5 (1962) 176.Google Scholar
  42. 42.
    Goldbrecht, K. Hamann and G. Willers, Journal of Physics E: Scientific Instruments, 4 (1971) 21.CrossRefGoogle Scholar
  43. 43.
    Reading, D. Elliott and V.L. Hill, Proc. NATAS (1992) 145.Google Scholar
  44. 44.
    Reading, Trends in Polymer Science, 1 (1993) 8.Google Scholar
  45. 45.
    A.A. Lacey, C. Nikolopoulos, and M. Reading, 50 (1997) 279.Google Scholar
  46. 46.
    P. Haines, C. Keattch and M. Reading, Differential Scanning Calorimetry, Handbook of Thermal Analysis, (Ed.) M. Brown, Elsevier (1998).Google Scholar
  47. 47.
    D.M. Price, Thermochim. Acta, 315 (1998) 11.CrossRefGoogle Scholar
  48. 48.
    M. Reading, US Patent 5,474,385 (1995).Google Scholar
  49. 49.
    Reading, US Patent 5,474,385 (1995).Google Scholar
  50. 50.
    G.M.B. Parkes, P.A. Barnes and E.L. Charsley, Analytical Chemistry, 71 (13) (1999) 2482–2487.CrossRefGoogle Scholar
  51. 51.
    B. Schenker and R. Riesen. User Com. Information for Users of Mettler Toledo Thermal Analysis Systems, Dec. 1997, 10–12.Google Scholar
  52. 52.
    G.M. Parkes, et al. Thermochimica Acta, 354 (2000) 39–43.CrossRefGoogle Scholar
  53. 53.
    M. Reading, Handbook of Thermal Analysis and Calorimetry (Chapter 8), (Ed.) M.E. Brown, 1998: Elsevier. G.M.B. Parkes.Google Scholar
  54. 54.
    G.M.B. Parkes, P.A. Barnes, and E.L. Charsley, Analytical Chemistry. 71 (13) (1999) 2482–2487.CrossRefGoogle Scholar
  55. 55.
    J. Opfermann, Netzsch Geraetebau, Germany-private communication.Google Scholar
  56. 56.
    M. Reading, Thermal Analysis — Techniques and Applications, (Eds.) E.L. Charsley and S.B. Warrington, Royal Society of Chemistry, Cambridge.Google Scholar
  57. 57.
    P.S. Gill, S.R. Sauerbrunn and B.S. Crove, J. Thermal Anal., 38 (1992) 255–266.CrossRefGoogle Scholar
  58. 58.
    P.A. Barnes, G.M.B. Parkes and E.L. Charsley, Anal. Chem., 66 (1994) 2226.CrossRefGoogle Scholar
  59. 59.
    E.L. Charsley, C. Stewart, P.A. Barnes and G.M.B. Parkes, Paper presented at the 11th International Congress on Thermal Analysis and Calorimetry, Philadelphia, USA, 1996.Google Scholar
  60. 60.
    J.H. McGill Polymer, 2 (1961) 221.CrossRefGoogle Scholar
  61. 61.
    E.L. Charsley and A.C.F. Kamp. Thermal Analysis, Vol. 1, (Ed.) H.G. Wiedemann, Birkhauser Verlag, 1972.Google Scholar
  62. 62.
    E.L. Charsley, A.C.F. Kamp and J.A. Rumsey, Thermal Analysis, Vol. 1, (Ed.) H.G. Wiedemann, Birkhauser Verlag, 1980, 285.Google Scholar
  63. 63.
    G.M. Parkes, P.A. Barnes, and E.L. Charsley, Thermochimica Acta, 1998, 320 (1–2) p. 297–301.CrossRefGoogle Scholar
  64. 64.
    E.A. Dawson et al., Thermochimica Acta, 335 (1–2), (1999) 141–146.CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media Dordrecht 2003

Authors and Affiliations

  • J. Rouquerol
    • 1
  • O. Toft Sorensen
    • 2
  • P. Barnes
    • 3
  • E. L. Charsley
    • 3
  • E. Fesenko
    • 3
  • M. Reading
    • 4
  1. 1.Madirel LaboratoryCNRS-Université de ProvenceMarseilleFrance
  2. 2.Risoe National LaboratoryRoskildeDenmark
  3. 3.Materials DepartmentUniversity of HuddersfieldUK
  4. 4.IPTMELoughborough UniversityLoughboroughUK

Personalised recommendations