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The Use of Thin-Layer Chromatography With Infrared Spectroscopy

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Developments in Applied Spectroscopy

Part of the book series: Developments in Applied Spectroscopy ((DAIS,volume 3))

Abstract

Thin-layer chromatography is a fast and economical way of separating mixtures of non-volatile liquids or solids. It requires only a small amount of sample and is applicable to problems in diversified fields. It serves as a useful complement to column and paper chromatography, and, like these methods, it requires some other analytical tool for positive identification of the separated components. In this work infrared spectroscopy has been used with thin-layer chromatography to analyze synthetic mixtures, organic reaction products, and commercial samples. Several techniques for obtaining IR spectra from the thin-layer spots will be described, and special methods of preparing the thin-layer plates will be recommended. The combined use of these two tools holds unique advantages and is certain to be employed even more frequently in the analytical and research laboratories.

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References

  1. R. S. Gohlke, Anal. Chem. 31:535 (1959).

    Article  CAS  Google Scholar 

  2. L. P. Lindeman and J. L. Annes, ibid. 32:1742 (1960).

    CAS  Google Scholar 

  3. A. A. Ebert, Jr., ibid. 33:1865 (1961).

    CAS  Google Scholar 

  4. R. A. Brown and E. R. Quiram, Appl. Spectroscopy 17:33 (1963).

    Article  CAS  Google Scholar 

  5. W. I. Kaye, Fifth International Instruments and Measurements Conference, Stockholm, September, 1960.

    Google Scholar 

  6. J. Haslam, A. R. Jeffs, and H. A. Willis, Analyst 86:44 (1961).

    Article  CAS  Google Scholar 

  7. W. S. Callaway, T. Johns, D. G. Tipotsch, and W. F. Ulrich, Pittsburgh Conference on Analytical Chemistry and Applied Spectroscopy, March, 1958.

    Google Scholar 

  8. R. V. Helm, D. R. Latham, C. R. Ferrin, and J. S. Ball, Anal. Chem. 32:1765 (1960).

    Article  CAS  Google Scholar 

  9. J. G. Grasselli and M. K. Snavely, Appl. Spectroscopy 16:190 (1962).

    Article  Google Scholar 

  10. M. Cachia, J. Appl. Chem. 8:291 (1958).

    Article  CAS  Google Scholar 

  11. R. Bravo and F. Hernandez, J. Chromatog. 7:60 (1962).

    Article  Google Scholar 

  12. H. L. Bird Jr., H. F. Brickley, J. P. Comer, P. E. Hartsaw, and M. L. Johnson, Anal. Chem. 35:346 (1963).

    Article  CAS  Google Scholar 

  13. J. H. Dhont and C. DeRooy, Analyst 86:74 (1961).

    Article  CAS  Google Scholar 

  14. K. Heyns and H F. Grützmacher, Angew. Chem. Intern, Ed. Engl. 1:400 (1962).

    Article  Google Scholar 

  15. N.A. Ismailov and M.S. Schraiber, Farmatsiya 3:1 (1938).

    Google Scholar 

  16. E. Stahl, Arch. Pharm. 292:411 (1959).

    Article  CAS  Google Scholar 

  17. E. Stahl, Chemiker Ztg. 82:323 (1958).

    CAS  Google Scholar 

  18. E. Stahl, Fette, Seifen, Anstrichmittel 60:1027 (1958).

    Google Scholar 

  19. E. Stahl, Parfue. Kosmetik. 39:564 (1958).

    Google Scholar 

  20. E. Stahl, Pharm. Rundschau. 1 No. 2 (1959).

    Google Scholar 

  21. E. Stahl, Pharm. Weekblad. 92:829 (1957).

    CAS  Google Scholar 

  22. R. Wasicky, Anal. Chem. 34:1346 (1962).

    Article  Google Scholar 

  23. F. J. Ritter and G. M. Meyer, Nature 193:941 (1962).

    Article  CAS  Google Scholar 

  24. T.M. Lees and P.J. DeMuria, J. Chromatog. 8:108 (1962).

    Article  CAS  Google Scholar 

  25. G.R. Duncan, ibid. 8:37 (1962).

    Article  CAS  Google Scholar 

  26. E. A. Mistryukov, ibid. 9:311 (1962).

    CAS  Google Scholar 

  27. E. G. Wollish, M. Schmall, and M. Hawrylshyn, Anal. Chem. 33:1138 (1961).

    Article  CAS  Google Scholar 

  28. M. E. Morgan, J. Chromatog. 9:379 (1962).

    Article  CAS  Google Scholar 

  29. R. D. Spencer and B. H. Beggs, Pittsburgh Conference on Analytical Chemistry and Applied Spectroscopy, March, 1963.

    Google Scholar 

  30. J. M. Augl and A. A. Buss, Cleveland Section A. C. S., Meeting-In-Miniature, December 19, 1962.

    Google Scholar 

  31. D. P. Tate, J. M. Augl, A. A. Buss, Inorg. Chem. 2:427 (1963).

    Article  CAS  Google Scholar 

  32. R. Poilblanc and M. Bigorgne, Bull. Soc. Chim. France, 1301 (1962).

    Google Scholar 

  33. D. P. Tate, J. M. Augl, A. A. Buss, B. L. Ross, and J. G. Grasselli (in manuscript).

    Google Scholar 

  34. W. H. Shumaker, Chemist-Analyst 50:22 (1961).

    CAS  Google Scholar 

  35. W. H. Shumaker (private communication).

    Google Scholar 

  36. H. L. Sloane, Pittsburgh Conference on Analytical Chemistry and Applied Spectroscopy, March, 1962.

    Google Scholar 

  37. S. M. Rybicka, Chem. Ind. 7:308 (1962).

    Google Scholar 

  38. J. A. Thoma, Anal. Chem. 35:215 (1963).

    Article  Google Scholar 

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© 1964 Chicago Section of the Society for Applied Spectroscopy

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Snavely, M.K., Grasselli, J.G. (1964). The Use of Thin-Layer Chromatography With Infrared Spectroscopy. In: Forrette, J.E., Lanterman, E. (eds) Developments in Applied Spectroscopy. Developments in Applied Spectroscopy, vol 3. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-8688-9_10

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  • DOI: https://doi.org/10.1007/978-1-4684-8688-9_10

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4684-8690-2

  • Online ISBN: 978-1-4684-8688-9

  • eBook Packages: Springer Book Archive

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