Skip to main content

An NMR Study of Acrylic Polymers

  • Chapter
Developments in Applied Spectroscopy

Part of the book series: Developments in Applied Spectroscopy ((DAIS,volume 7b))

  • 197 Accesses

Abstract

Solvent chemical-shift and temperature effects on acrylic-copolymers were studied. The solvents used in this investigation were o-dichlorobenzene, bromoform, 1,1,2,2-tetrachloroethylene, and 1,1,2,2-tetrabromoethane. Bromoform was found to give the best resolved spectra at a temperature of 102 C. Analytical data obtained by integration of the NMR resonance bands for the arcylic copolymers were within a few percent of the initial monomer content.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

eBook
USD 16.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 16.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. K. J. Liu, J. Polymer Sci. Part A-2 5, 1199 (1967).

    CAS  Google Scholar 

  2. K. J. Liu, J. S. Szutz, and R. Ullman, Am. Chem. Soc, Div. Polymer Chem., Preprints 5 (2), 761 (1964).

    CAS  Google Scholar 

  3. A. Nishioka, H. Watanabe, I. Yamagushi, and H. Shimizu, J Polymer Sci. 45, 323 (1960).

    Google Scholar 

  4. T. Yoshino, Y. Kikuchi, and J. Komiyama, J. Phys. Chem. 70(4), 1059 (1966).

    Article  CAS  Google Scholar 

  5. U. Johnsen, Kolloid Z. 178, 161 (1961).

    Article  CAS  Google Scholar 

  6. L. J. Merrill, J. A. Sauer, and A. E. Woodward, J. Polymer Sci. Part A 3(12), 4243 (1965).

    CAS  Google Scholar 

  7. K. Matsuzaki, T. Uryn, A. Ishida, and T. Ohki, J. Polymer Sci. Part B 2(12), 1139 (1964).

    Article  Google Scholar 

  8. J. G. Powles, J. H. Strange, and D. J. H. Sandiford, Polymer 4(3), 401 (1963).

    Article  CAS  Google Scholar 

  9. N. M. Bazhenov, M. V. Vol’kenshtein, and A. S. Khachaturov, Vysokomolekul. Soedin. 5(7), 1025 (1963).

    CAS  Google Scholar 

  10. F. A. Bovey, J. Polymer Sci. 46(147), 59 (1960).

    Article  CAS  Google Scholar 

  11. A. Nishioka, Y. Kato, T. Vetake, and H. Watanabe, J. Polymer Sci. 61, S32–S33 (1962).

    Article  Google Scholar 

  12. H. Watanabe, Y. Kato, and A. Nishioka, Kogyo Kagaku Zasshi 65, 270 (1962).

    Article  CAS  Google Scholar 

  13. M. L. Miller and C. E. Rauhut, J. Polymer Sci. 38(133), 63 (1959).

    Article  CAS  Google Scholar 

  14. K. M. Sinnott, J. Polymer Sci. 42, 3 (1960).

    Article  CAS  Google Scholar 

  15. N. Grassie, B. J. D. Torrance, J. D. Fortune, and J. D. Gemmell, Polymer 6, 653 (1965).

    Article  CAS  Google Scholar 

  16. F. A. Bovey, J. Polymer Sci. 62, 197 (1962).

    Article  CAS  Google Scholar 

  17. K. C. Ramey and J. Messiek, J. Polymer Sci. Part A-2 4, 155 (1961).

    Article  Google Scholar 

  18. C. Haney, F. A. Johnson, and M. G. Baldwin, J. Polymer Sci. Part A 4(7), 1791 (1966).

    Article  CAS  Google Scholar 

  19. H. A. Willis and M. E. A. Cudby, Appl. Spectry. Rev. 1 (2), 237 (1968).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1970 Chicago Section of the Society for Applied Spectroscopy

About this chapter

Cite this chapter

Netzel, D.A. (1970). An NMR Study of Acrylic Polymers. In: Grove, E.L., Perkins, A.J. (eds) Developments in Applied Spectroscopy. Developments in Applied Spectroscopy, vol 7b. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-8589-9_13

Download citation

  • DOI: https://doi.org/10.1007/978-1-4684-8589-9_13

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4684-8591-2

  • Online ISBN: 978-1-4684-8589-9

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics