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Applications of Multinuclear NMR in the Solid State to Structural and Dynamical Problems in Macromolecular Chemistry

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NMR Applications in Biopolymers

Part of the book series: Basic Life Sciences ((BLSC,volume 56))

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Abstract

Nuclear magnetic resonance is a long established molecular spectroscopy that provides both dynamical and structural information about the molecules bearing the nuclear spin observed. Currently, data acquisition is accomplished in the time domain by the application of radio frequency excitation followed by acquisition of the transient nuclear induction signal using rapid analog to digital conversion for storage of the data set in a fast and usually dedicated digital computer. A Fourier transform of the time domain signal provides the usual frequency domain spectrum that is most often interpreted to yield structural information about the molecules observed.

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References

  • Abragam, A., 1961, Principles of Nuclear Magnetism, Clarendon Press, Oxford, Ch. 7.

    Google Scholar 

  • Azuory, R., Aronhime, J. S., Sarig, S., Abrashkin, S., Mayer, I., and Garti, N., 1988, J. Am. Oil Chem. Soc., a6:964.

    Article  Google Scholar 

  • Bociek, S. M., Ablatt, S., and Norton, I. T., 1985, J. Am. Oil Chem. Soc., 62:1261.

    Article  CAS  Google Scholar 

  • Burnett, L. J., and Muller, B. H., 1971, J. Chem. Phys., 55:5829.

    Article  CAS  Google Scholar 

  • Davis, J. H., 1983, Biochem. Biophys. Acta., 737:117.

    PubMed  CAS  Google Scholar 

  • Derbyshire, V., Gorvin, T. C., and Warner, D., 1969, Mol. Phys., 17:401.

    Article  CAS  Google Scholar 

  • Dudley, R. L., and Fyfe, C. A., 1982, Fuel, 61:651.

    Article  CAS  Google Scholar 

  • Ernst, R. R., Bodenhausen, G., and Wokaun, A., 1987, “Principles of Nuclear Magnetic Resonance In One and Two Dimensions,” Clarendon Press, Oxford.

    Google Scholar 

  • Fyfe, C. A., 1983, Solid State NMR for Chemists, C.F.C. Press, (P.O. Box 1720, Guelph, Ontario, Canada).

    Google Scholar 

  • Gerstein, B. C., and Dybowski, C. R., 1985, Transient Techniques in NMR of Solids, Academic Press, New York.

    Google Scholar 

  • Gibon, V., Durant, F., and Deroanne, C., 1986, J. Am. Oil Chem. Soc., 63:1047.

    Article  CAS  Google Scholar 

  • Gorenstein, D. G., ed., 1984, Phosphorus-31 NMR, Academic Press, New York.

    Google Scholar 

  • Griffin, R. G., 1981, Methods in Enzymology, 72:108.

    Article  PubMed  CAS  Google Scholar 

  • Jackson, C. L., and Bryant, R. G., 1989, Biochemistry, 28:5024.

    Article  PubMed  CAS  Google Scholar 

  • Jacob, G. S., Schaefer, J., and Wilson, Jr., G. E., 1985, J. Biol. Chem., 260:2777.

    PubMed  CAS  Google Scholar 

  • Jelinski, L. W., 1986, “High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk,” R. A. Komoroski, ed., VCH Publishers, Deerfield Beach, Florida, p. 335.

    Google Scholar 

  • Kennedy, S. D., and Bryant, R. G., 1990, Biopolymers, in press.

    Google Scholar 

  • Komoroski, R. A., and Mandelkern, L., 1986, High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk, R.A. Komoroski, ed., VCH Publishers, Deerfield Beach, Florida, pp. 1–17.

    Google Scholar 

  • Kunts, I. D., and Kauzman, W., 1974, Adv. Protein Chem., 28:239.

    Article  Google Scholar 

  • Larsson, K., 1964, Ark. Kemi., 23:1.

    CAS  Google Scholar 

  • Mehring, M., 1976, High Resolution NMR Spectroscopy in Solids, Springer-Verlag Series: NMR Basic Principles and Progress, Volume 11.

    Google Scholar 

  • Norton, I. T., Lee-Tuffnell, C. D., Ablett, S., and Bociek, S. M., 1985, J. Am. Oil Chem. Soc., 62:1237.

    Article  CAS  Google Scholar 

  • Small, D. M., 1986, “The Physical Chemistry of Lipids, from Alkanes to Phospholipids,” V. 4 in Handbook of Lipid Research, Plenum Press, New York, pps. 26–7 for hydrocarbon chain packing volumes.

    Google Scholar 

  • Smith, R. L., and Oldfield, E., 1984, Science, 225:280.

    Article  PubMed  CAS  Google Scholar 

  • Spiess, H. W., 1985, Adv. Polymer Sci., 66:24.

    Google Scholar 

  • Torchia, D. A., and Szabo, A., 1982, J. Magn. Reson., 107.

    Google Scholar 

  • Wuthrich, K., et al., 1989, J. Am. Chem. Soc., 111:1871.

    Article  Google Scholar 

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© 1990 Plenum Press, New York

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Bryant, R.G., Kennedy, S.D., Jackson, C.L., Eads, T.M., Croasmun, W.R., Blaurock, A.E. (1990). Applications of Multinuclear NMR in the Solid State to Structural and Dynamical Problems in Macromolecular Chemistry. In: Finley, J.W., Schmidt, S.J., Serianni, A.S. (eds) NMR Applications in Biopolymers. Basic Life Sciences, vol 56. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-5868-8_14

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  • DOI: https://doi.org/10.1007/978-1-4684-5868-8_14

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4684-5870-1

  • Online ISBN: 978-1-4684-5868-8

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