Skip to main content

A Furnace for Molten Salt Raman Spectroscopy to 800°C

  • Chapter
  • 321 Accesses

Abstract

Molten fluorides are usually extremely corrosive towards conventional optical window material; therefore, generally it is not feasible to use these materials in fabricating cells to measure the Raman spectra of fluoride melts. However, both windowless1 and diamond window2 cells have been developed for measuring the visible and uv absorption spectra of molten fluorides. Modifications of these cells are suitable for laser-Raman spectroscopy; the present article describes a furnace designed especially for use with either of the two types of cells mentioned above. The furnace also can be used with more conventional types of sample contaminent cells.

This is a preview of subscription content, log in via an institution.

Buying options

Chapter
USD   29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD   39.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD   54.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Learn about institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Reference

  1. J. P. Young, Anal. Chem. 36, 390 (1964).

    Article  CAS  Google Scholar 

  2. L. M. Toth, J. P. Young, and G. P. Smith, Anal. Chem. 41, 683 (1969).

    Article  CAS  Google Scholar 

  3. J. P. Young and J. C. White, Anal. Chem. 31, 1892 (1959).

    Article  CAS  Google Scholar 

  4. J. P. Young, Oak Ridge National Laboratory Analytical Chemistry Division Annual Progress Report, ORNL-3537, 15 Nov. 1963, p. 26.

    Google Scholar 

  5. J. P. Young, Inorg. Chem. 6, 1486 (1967).

    Article  CAS  Google Scholar 

  6. V. A. Maroni and E. J. Cairns, in Molten Salts: Characterization and Analysis, edited by G. Mamantov ( Marcel Dekker, New York, 1969 ), p. 231.

    Google Scholar 

  7. J. H. R. Clarke and R. E. Hester, J. Chem. Phys. 50, 3106 (1969).

    Article  CAS  Google Scholar 

  8. F. F. Neale and R. E. Thurstans, J. Sci. Instrum. (J. Phys. E) (Ser. 2 ), 2, 898 (1969).

    Article  Google Scholar 

  9. M. H. Brooker, A. S. Quist, and G. E. Boyd, Chem. Phys. Lett. 5, 357 (1970).

    Article  CAS  Google Scholar 

  10. A. S. Quist, J. B. Bates, and G. E. Boyd, Oak Ridge National Laboratory Chemistry Division Annual Progress Report, ORNL-4581, 20 May 1970.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1974 Springer Science+Business Media New York

About this chapter

Cite this chapter

Quist, A.S. (1974). A Furnace for Molten Salt Raman Spectroscopy to 800°C. In: May, L. (eds) Spectroscopic Tricks. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-2742-4_61

Download citation

  • DOI: https://doi.org/10.1007/978-1-4684-2742-4_61

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4684-2744-8

  • Online ISBN: 978-1-4684-2742-4

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics