Abstract
Molten fluorides are usually extremely corrosive towards conventional optical window material; therefore, generally it is not feasible to use these materials in fabricating cells to measure the Raman spectra of fluoride melts. However, both windowless1 and diamond window2 cells have been developed for measuring the visible and uv absorption spectra of molten fluorides. Modifications of these cells are suitable for laser-Raman spectroscopy; the present article describes a furnace designed especially for use with either of the two types of cells mentioned above. The furnace also can be used with more conventional types of sample contaminent cells.
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Reference
J. P. Young, Anal. Chem. 36, 390 (1964).
L. M. Toth, J. P. Young, and G. P. Smith, Anal. Chem. 41, 683 (1969).
J. P. Young and J. C. White, Anal. Chem. 31, 1892 (1959).
J. P. Young, Oak Ridge National Laboratory Analytical Chemistry Division Annual Progress Report, ORNL-3537, 15 Nov. 1963, p. 26.
J. P. Young, Inorg. Chem. 6, 1486 (1967).
V. A. Maroni and E. J. Cairns, in Molten Salts: Characterization and Analysis, edited by G. Mamantov ( Marcel Dekker, New York, 1969 ), p. 231.
J. H. R. Clarke and R. E. Hester, J. Chem. Phys. 50, 3106 (1969).
F. F. Neale and R. E. Thurstans, J. Sci. Instrum. (J. Phys. E) (Ser. 2 ), 2, 898 (1969).
M. H. Brooker, A. S. Quist, and G. E. Boyd, Chem. Phys. Lett. 5, 357 (1970).
A. S. Quist, J. B. Bates, and G. E. Boyd, Oak Ridge National Laboratory Chemistry Division Annual Progress Report, ORNL-4581, 20 May 1970.
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© 1974 Springer Science+Business Media New York
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Quist, A.S. (1974). A Furnace for Molten Salt Raman Spectroscopy to 800°C. In: May, L. (eds) Spectroscopic Tricks. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-2742-4_61
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DOI: https://doi.org/10.1007/978-1-4684-2742-4_61
Publisher Name: Springer, Boston, MA
Print ISBN: 978-1-4684-2744-8
Online ISBN: 978-1-4684-2742-4
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