A Simple System for Transferring Air-Sensitive Compounds into Capillaries from Schlenk Tubes
Our organoactinide research has produced a number of extremely air-sensitive compounds. Experimental difficulties have been encountered during the transfer of these air-sensitive compounds from Schlenk tubes1 into capillary tubes for mass spectral analysis. To overcome these experimental difficulties, a simple transfer device (see Fig. 1) has been designed.
KeywordsCapillary Tube Experimental Difficulty Atomic Energy Commission Mass Spectral Analysis Schlenk Tube
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- 1.D. F. Shriver, The Manipulation of Air-Sensitive Compounds ( McGraw-Hill, New York, 1969 ), pp. 141–155.Google Scholar