Abstract
Our organoactinide research has produced a number of extremely air-sensitive compounds. Experimental difficulties have been encountered during the transfer of these air-sensitive compounds from Schlenk tubes1 into capillary tubes for mass spectral analysis. To overcome these experimental difficulties, a simple transfer device (see Fig. 1) has been designed.
Work performed under U. S. Atomic Energy Commission Contract AT(29-1)-1106.
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References
D. F. Shriver, The Manipulation of Air-Sensitive Compounds ( McGraw-Hill, New York, 1969 ), pp. 141–155.
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© 1974 Springer Science+Business Media New York
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Eggerman, W.G. (1974). A Simple System for Transferring Air-Sensitive Compounds into Capillaries from Schlenk Tubes. In: May, L. (eds) Spectroscopic Tricks. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-2742-4_45
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DOI: https://doi.org/10.1007/978-1-4684-2742-4_45
Publisher Name: Springer, Boston, MA
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