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Prevention of Laser Microprobe Staining of Analyzed Metals

  • H. N. Barton
  • J. Benallo

Abstract

The laser microprobe is a useful tool for the analysis of specific sample areas of approximately 50 μ diameter. The auxiliary spark excitation of Brech and Cross1 increases spectrum intensity but results in a staining of metal sample surfaces in the area of analysis.2 Sample surface detail is thus obscured and selection of analysis sites for subsequent determinations is extremely difficult. The capability of the laser microprobe to selectively sample closely adjacent areas is thereby nullified. Deposition of the stain can be restricted to the dimensions of a central hole in a paper shield; however, placement of a shield is difficult even for plane surface samples.

Keywords

Central Hole Stainless Steel Tubing Atomic Energy Commission Analysis Site Surface Detail 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Reference

  1. 1.
    F. Brech and L. Cross, Abstracts of Xth Colloquium Spectroscopium Internationale and First Meeting of the Society for Applied Spectroscopy, Appl. Spectrosc. 16, 59 (1962).Google Scholar
  2. 2.
    S. D. Rasberry, B. F. Scribner and M. Margoshes, Appl. Opt. 6, 81 (1967).Google Scholar
  3. 3.
    Collodion, U. S. P., J. T. Baker 9209, J. T. Baker Co., Phillipsburg, N. J.Google Scholar
  4. 1.
    E. A. Boling, Spectrochim. Acta 22, 425 (1966).Google Scholar

Copyright information

© Springer Science+Business Media New York 1974

Authors and Affiliations

  • H. N. Barton
    • 1
  • J. Benallo
    • 1
  1. 1.Rocky Flats DivisionThe Dow Chemical CompanyGoldenUSA

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