Abstract
In order to determine boron in the borides of refractory metals as well as in ores, minerals, and steels containing more than 0.2% of this element, a classical volumetric method of titration with a solution of caustic soda in the presence of glycerin or mannitol is often employed [1,2,6]. For determining boron in quantities of under 0.05% colorimetric methods are used; these incorporate quinalizarin, carminic acid, arsenazo I, and so on, the reaction with boron taking place in concentrated sulfuric acid [1,4,7].
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Literature Cited
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Nikitina, E.I. (1972). Photometric Determination of Boron in Nickel and Titanium Borides Using Magnezone I in an Alkaline Medium. In: Samsonov, G.V. (eds) Chemical Properties and Analysis of Refractory Compounds / Khimicheskie Svoistva I Metody Analiza Tugoplavkikh Soedinenii / Химические Свойства И Методы Анализа Тугоплавких Соединений. Springer, Boston, MA. https://doi.org/10.1007/978-1-4615-8555-8_21
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DOI: https://doi.org/10.1007/978-1-4615-8555-8_21
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