Skip to main content
  • 116 Accesses

Abstract

In order to determine boron in the borides of refractory metals as well as in ores, minerals, and steels containing more than 0.2% of this element, a classical volumetric method of titration with a solution of caustic soda in the presence of glycerin or mannitol is often employed [1,2,6]. For determining boron in quantities of under 0.05% colorimetric methods are used; these incorporate quinalizarin, carminic acid, arsenazo I, and so on, the reaction with boron taking place in concentrated sulfuric acid [1,4,7].

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 39.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 54.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Literature Cited

  1. W. F. Hillebrand et al., Practical Handbook on Inorganic Analysis [Russian translation], Yu. Yu. Lur’e, ed., Goskhimizdat (1957).

    Google Scholar 

  2. A. M. Dymov, Technical Analysis of Ores and Metals [in Russian], Metallurgizdat, Moscow (1949).

    Google Scholar 

  3. G. V. Samsonov et al., Analysis of Refractory Compounds [in Russian], Metallurgizdat, Moscow (1962).

    Google Scholar 

  4. Z. S. Mukhina and A. F. Aleshina, Zavod. Lab., No. 1 (1945).

    Google Scholar 

  5. F. Faigel, Drop Analysis [Russian translation], Goskhimizdat, Moscow (1933).

    Google Scholar 

  6. I. M. Korenman, Zh. Analit. Khim., 2 (3): 153 (1947).

    CAS  Google Scholar 

  7. N. S. Poluéktov and N. P. Nikonov, in: Transactions of the Commission on Analytical Chemistry, Vol. 3, Izd. AN SSSR, Moscow (1951), p. 4.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1972 Consultants Bureau, New York

About this chapter

Cite this chapter

Nikitina, E.I. (1972). Photometric Determination of Boron in Nickel and Titanium Borides Using Magnezone I in an Alkaline Medium. In: Samsonov, G.V. (eds) Chemical Properties and Analysis of Refractory Compounds / Khimicheskie Svoistva I Metody Analiza Tugoplavkikh Soedinenii / Химические Свойства И Методы Анализа Тугоплавких Соединений. Springer, Boston, MA. https://doi.org/10.1007/978-1-4615-8555-8_21

Download citation

  • DOI: https://doi.org/10.1007/978-1-4615-8555-8_21

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4615-8557-2

  • Online ISBN: 978-1-4615-8555-8

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics