Materials and Methods

  • Camille Petit
Part of the Springer Theses book series (Springer Theses)


A first series of samples was prepared by carbonization of different polymers with or without a subsequent oxidation treatment.


Graphite Titration Fourier Transform Infrared Spectroscopy Vanadate Sulfuric Acid 


  1. 1.
    D. Hines, et al., “Surface Properties of Porous CarbonCarbon Obtained from Polystyrene Sulfonic Acid-Based Organic Salts,” Langmuir, vol. 20, pp. 3388–3397, 2004.Google Scholar
  2. 2.
    C. Petit, et al., “The role of sulfur-containing groups in ammonia retention on activated carbons,” Carbon , vol. 48, pp. 654–667, 2010.Google Scholar
  3. 3.
    I. I. Salame and T. J. Bandosz, “Study of Water Adsorption on Activated Carbons with Different Degrees of Surface Oxidation,” Journal of Colloid and Interface Science, vol. 210, pp. 367–374, 1999.Google Scholar
  4. 4.
    C. Petit, et al., “Interactions of Ammonia with the Surface of Microporous Carbon Impregnated with Transition Metal Chlorides,” The Journal of Physical Chemistry C, vol. 111, pp. 12705–12714, 2007.Google Scholar
  5. 5.
    C. Petit and T. J. Bandosz, “Complexity of ammonia interactions on activated carbons modified with V2O5,” Journal of Colloid and Interface Science, vol. 325, pp. 301–308, 2008.Google Scholar
  6. 6.
    C. Petit and T. J. Bandosz, “Role of surface heterogeneity in the removal of ammonia from air on micro/mesoporous activated carbons modified with molybdenum and tungtsen oxides,” Microporous and Mesoporous Materials, vol. 118, pp. 61–67, 2009.Google Scholar
  7. 7.
    C. Petit and T. J. Bandosz, “Removal of Ammonia from Air on Molybdenum and Tungsten Oxide Modified Activated Carbons,” Environmental Science & Technology, vol. 42, pp. 3033–3039, 2008.Google Scholar
  8. 8.
    C. Petit and T. J. Bandosz, “Role of Aluminum Oxycations in Retention of Ammonia on Modified Activated Carbons,” The Journal of Physical Chemistry C, vol. 111, pp. 16445–16452, 2007.Google Scholar
  9. 9.
    C. Petit and T. J. Bandosz, “Activated carbons modified with aluminium-zirconium polycations as adsorbents for ammonia,” Microporous and Mesoporous Materials, vol. 114, pp. 137–147, 2008.Google Scholar
  10. 10.
    T. J. Bandosz, et al., “Surface acidity of pillared taeniolites in terms of their proton affinity distributions,” The Journal of Physical Chemistry, vol. 99, pp. 13522–13527, 1995.Google Scholar
  11. 11.
    W. S. Hummers and R. E. Offeman, “Preparation of Graphitic Oxide,” Journal of the American Chemical Society, vol. 80, pp. 1339–1339, 1958.Google Scholar
  12. 12.
    M. B. C. Brodie, “Sur le poids atomique du graphite,” Ann. Chim. Phys., vol. 59, pp. 466–472, 1860.Google Scholar
  13. 13.
    U. Mueller, et al., “Metal-organic frameworks-prospective industrial applications,” Journal of Materials Chemistry, vol. 16, pp. 626–636, 2006.Google Scholar
  14. 14.
    O. M. Yaghi, et al., “Reticular synthesis and the design of new materials,” Nature, vol. 423, pp. 705–714, 2003.Google Scholar
  15. 15.
    O. M. Yaghi. MOF-5 network. Available:
  16. 16.
    S. S.-Y. Chui, et al., “A Chemically Functionalizable Nanoporous Material [Cu3(TMA)2(H2O)3]n,” Science, vol. 283, pp. 1148–1150, 1999.Google Scholar
  17. 17.
    T. Cassagneau, et al., “Preparation and Characterization of Ultrathin Films Layer-by-Layer Self-Assembled from Graphite Oxide Nanoplatelets and Polymers,” Langmuir, vol. 16, pp. 7318–7324, 2000.Google Scholar
  18. 18.
    Y. Song, et al., “Synthesis of polyoxometalates-functionalized carbon nanotubes composites and relevant electrochemical properties study,” Materials Research Bulletin, vol. 42, pp. 1485–1491, 2007.Google Scholar
  19. 19.
    Z.-H. Liu, et al., “Intercalation of Organic Ammonium Ions into Layered Graphite Oxide,” Langmuir, vol. 18, pp. 4926–4932, 2002.Google Scholar
  20. 20.
    T. Szabó, et al., “Enhanced acidity and pH-dependent surface charge characterization of successively oxidized graphite oxides,” Carbon , vol. 44, pp. 537–545, 2006.Google Scholar
  21. 21.
    M. J. Janik, et al., “A computational and experimental study of anhydrous phosphotungstic acid and its interaction with water molecules,” Applied Catalysis A: General, vol. 256, pp. 51–68, 2003.Google Scholar
  22. 22.
    Wkipedia. Phosphotungstic acid. Available:
  23. 23.
    C. Petit and T. J. Bandosz, “MOF–Graphite Oxide Composites: Combining the Uniqueness of Graphene Layers and Metal–Organic Frameworks,” Advanced Materials, vol. 21, pp. 4753–4757, 2009.Google Scholar
  24. 24.
    C. Petit and T. J. Bandosz, “The synthesis and characterization of copper-based metal organic framework/graphite oxide composites,” Carbon , vol. 49, pp. 563–572, 2011.Google Scholar
  25. 25.
    M. M. Dubinin, Ed., Chemistry and physics of carbon. New York: Dekker, 1966, p.^pp. Pages.Google Scholar
  26. 26.
    C. Lastoskie, et al., “Pore size distribution analysis of microporous carbons: a density functional theory approach,” The Journal of Physical Chemistry, vol. 97, pp. 4786–4796, 1993.Google Scholar
  27. 27.
    J. Jagiello, “Stable Numerical Solution of the Adsorption Integral Equation Using Splines,” Langmuir, vol. 10, pp. 2778–2785, 1994.Google Scholar
  28. 28.
    J. Jagiello, et al., “Carbon surface characterization in terms of its acidity constant distribution,” Carbon, vol. 32, pp. 1026–1028, 1994.Google Scholar

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© Springer Science+Business Media New York 2012

Authors and Affiliations

  • Camille Petit
    • 1
  1. 1.Department of ChemistryCUNY—City University of New YorkNew YorkUSA

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