Abstract
The study of species sorbed to surfaces is a daunting experimental problem. Numerous techniques have from time-to-time been developed which have provided information but few would suggest that our current state of knowledge is better than sparse. The classical techniques involve:
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a)
The measurement of vapour pressures of volatiles over surfaces as a function of temperature and mass of species sorbed and
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b)
Desorption (by pumping and heating) followed by chemical or physical analyses of the desorbed species.
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Bibliography
Infrared spectra of adsorbed species
L. H. Little, Infrared Spectra of Adsorbed Species, 1966, Academic Press, N.Y.
Experimental developments: “Surface Adsorbed Samples” by N. D. Parkyns, Chapter in Lab. Methods in Infrared Spectroscopy”, Ed. R. G. Miller and B. C. Stone, 2nd Edn. Keyden, London 1972.
Reviews on Raman Spectroscopy of Sorbed Species
R. P. Cooney, G. Curthoys and N. T. Tam, Advances in Cat., 24, 293 (1975).
R. L. Paul and P. J. Hendra, Minerals. Sci. Engng. 8, 171 (1976); and references cited therein.
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© 1978 Plenum Press, New York
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Hendra, P.J., Fleischmann, M. (1978). Raman Spectroscopy at Surfaces. In: Kay, E., Bagus, P.S. (eds) Topics in Surface Chemistry. The IBM Research Symposia Series. Springer, Boston, MA. https://doi.org/10.1007/978-1-4613-4003-4_15
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DOI: https://doi.org/10.1007/978-1-4613-4003-4_15
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