Abstract
This research is based on high performance liquid chromatographic method for the determination of bisphenol A, nonylphenol and octylphenol in sewage. Sewage samples use dispersive liquid–liquid extraction-pre column derivatization-High performance liquid chromatography method for the determination. Dichloromethane is extracting agent. Acetonitrile and water (V:V = 90:10) are mobile phase. Bisphenol A, nonylphenol and octylphenol detect by Inertsil ODS-P column (5 μm, 250 × 4.6 mm) after the separation of fluorescence. Fluorescence excitation wavelength is 227 nm. The emission wavelength is 313 nm. Sample complete in 6 min within the peak. Linear range is 0.1−10 mg/L. In 0.1, 0.5 and 1 mg/L three concentrations of added level of sewage recovery of samples are respectively 94.7–106.8 %. The method is simple, rapid and economic actual samples. It can be used for sewage.
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References
Xiao J, Shao B, Wu XY et al (2011) A study on bisphenol A, nonylphenol, and octyphenol in human urine amples detected by SPE-UPLC-MS. Biomed Environ Sci 24(1):40–46
Cooper JE, Kendig EL, Belcher SM (2011) Assessment of bisphenol A released from reusable plastic, aluminium and stainless steel water bottles. Chemosphere 85(6):943–947
Yiantzi E, Psillakis E, Tyrovola K et al (2010) Vortex-assisted liquid–liquid microextraction of octylphenol, nonylphenol and bisphenol A. Talanta 80(5):2057–2062
Langdon KA, Warne MSJ, Smernik RJ et al (2011) Degradation of 4-nonylphenol, 4-t-octyphenol, bisphenol A and triclosan following biosolids addition to soil under laboratory conditions. Chemosphere 84(11):1556–1562
Zhou Q, Gao Y, Xie G (2011) Determination of bisphenol A, 4-n-nonylphenol, and 4-tert-octyphenol by temperature-controlled ionic liquid dispersive liquid-phase microextraction combined with high performance liquid chromatography-fluorescence detector. Talanta 85(3):1598–1602
Ferrer E, Santoni E, Vittori S et al (2011) Simultaneous determination of bisphenol A, octyphenol, and nonylphenol by pressurized liquid extraction and liquid chromatography tandem mass spectrometry in powdered milk and infant formulas. Food Chem 126(1):360–367
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© 2013 Springer-Verlag London
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Qian, Q., Cao, X., Wang, Q., Cao, Y., Rong, S., Yu, S. (2013). High-Performance Liquid Chromatographic Method for the Determination of Bisphenol A, Nonylphenol and Octylphenol in Sewage. In: Du, W. (eds) Informatics and Management Science I. Lecture Notes in Electrical Engineering, vol 204. Springer, London. https://doi.org/10.1007/978-1-4471-4802-9_91
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DOI: https://doi.org/10.1007/978-1-4471-4802-9_91
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