Abstract
Methods for characterizing edible lipids, fats, and oils can be separated into two categories: those developed to analyze bulk oils and fats, and those focusing on analysis of foodstuffs and their lipid extracts. In evaluating foodstuffs, it is usually necessary to extract the lipids prior to analysis. In these cases, if sufficient quantities of lipids are available, methods developed for bulk fats and oils can be utilized.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
AOAC International (2007) Official methods of analysis, 18th edn., 2005; Current through revision 2, 2007 (on-line). AOAC International, Gaithersburg, MD
AOCS (2009) Official methods and recommended practices of the AOCS, 6th edn. American Oil Chemists’ Society, Champaign, IL
IUPAC (1987) Standard methods for analysis of oils, fats, and derivatives and supplements, 7th edn. International Union of Pure and Applied Chemistry, Commission on Oils, Fats and Derivatives, Paquot C, Hautfenne A (eds). Blackwell Scientific, Oxford
Khanal RC, Dhiman TR (2004) Biosynthesis of conjugated linoleic acid (CLA): a review. Pak J Nutr 3:72–81
Christie WW (1982) Lipid analysis. Isolation, separation, identification, and structural analysis of lipids, 2nd edn. Pergamon, Oxford
Christie WW (1989) Gas chromatography and lipids. A practical guide. The Oily Press, Ayr, Scotland
Gray JI (1978) Measurement of lipid oxidation: a review. J Am Oil Chem Soc 55:539–546
Hamilton RJ, Rossell JB (1986) Analysis of oils and fats. Elsevier Applied Science, London
Melton SL (1983) Methodology for following lipid oxidation in muscle foods. Food Technol 37(7):105–111, 116
Pomeranz Y, Meloan CE (1994) Food analysis: theory and practice, 3rd edn. Chapman & Hall, New York
White PJ (1991) Methods for measuring changes in deep-fat frying oils. Food Technol 45(2):75–80
Hui YH (ed) (1996) Bailey’s industrial oil and fat products, 5th edn. Wiley, New York
Nawar WW (1996) Lipids, ch. 5. In: Fennema OR (ed) Food chemistry, 3rd edn. Marcel Dekker, New York
Budavari S (ed) (1996) The Merck index. An encyclopedia of chemicals, drugs, and biologicals, 12th edn. Merck, Whitehouse Station, NJ
Stauffer CE (1996) Fats and oils. Eagan Press handbook series. American Association of Cereal Chemists, St. Paul, MN
Labuza TP (1971) Kinetics of lipid oxidation in foods. CRC Crit Rev Food Technol 2:355–405
Buege JA, Aust SD (1978) Microsomal lipid peroxidation. Methods Enzymol 52:302–310
Fulcher RG, Irving DW, de Franciso A (1989) Fluorescence microscopy: applications in food analysis, ch. 3. In: Munck L (ed) Fluorescence analysis in foods. Longman Scientific & Technical, copublished in the U.S. with Wiley, New York, pp 59–109
Green FJ (1990) The Sigma-Aldrich handbook of stains, dyes and indicators. Aldrich Chemical, Milwaukee, WI
Smart MG, Fulcher RG, Pechak DG (1995) Recent developments in the microstructural characterization of foods, ch. 11. In: Gaonkar AG (ed) Characterization of food: emerging methods. Elsevier Science, New York, pp 233–275
Fritsch CW, Gale JA (1977) Hexanal as a measure of rancidity in low fat foods. J Am Oil Chem Soc 54:225
Dupey HP, Fore SP (1970) Determination of residual solvent in oilseed meals and flours: volatilization procedure. J Am Oil Chem Soc 47:231–233
Tarladgis BG, Watts BM, Younathan MT, Dugan LR (1960) A distillation method for the quantitative determination of malonaldehyde in rancid foods. J Am Oil Chem Soc 37:1
Rhee KS, Watts BM (1966) Evaluation of lipid oxidation in plant tissues. J Food Sci 31:664–668
Frankel EN (1993) In search of better methods to evaluate natural antioxidants and oxidative stability in food lipids. Trends Food Sci Technol 4:220–225
Perkins EG (1991) Analyses of fats, oils, and lipoproteins. American Oil Chemists’ Society, Champaign, IL
Schul D, Tallmadge D, Burress D, Ewald D, Berger B, Henry D (1998) Determination of fat in olestra-containing savory snack products by capillary gas chromatography. J AOAC Int 81:848–868
Tallmadge DH, Lin PY (1993) Liquid chromatographic method for determining the percent of olestra in lipid samples. J AOAC Int 76:1396–1400
Ackman RG, Sipos JC (1964) Application of specific response factors in the gas chromatographic analysis of methyl esters of fatty acids with flame ionization detectors. J Am Oil Chem Soc 41:377–378
Ratnayake WMN, Hansen SL, Kennedy MP (2006) Evaluation of the CP-Sil88 and SP-2560 GC columns used in the recently approved AOCS Official Method Ce 1h-05: determination of cis-, trans-, saturated, monounsaturated, and polyunsaturated fatty acids in vegetable or non-ruminant animal oils and fats by capillary GLC method. J Am Oil Chem Soc 83:475–488
Al-Hasani SM, Shabany H, Hlavac J (1990) Rapid determination of cholesterol in selected frozen foods. J Assoc Off Anal Chem 73:817–820
Adams ML, Sullivan DM, Smith RL, Richter EF (1986) Evaluation of direct saponification method for determination of cholesterol in meats. J Assoc Off Anal Chem 69:844–846
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
Copyright information
© 2010 Springer Science+Business Media, LLC
About this chapter
Cite this chapter
O’Keefe, S.F., Pike, O.A. (2010). Fat Characterization. In: Food Analysis. Food Analysis. Springer, Boston, MA. https://doi.org/10.1007/978-1-4419-1478-1_14
Download citation
DOI: https://doi.org/10.1007/978-1-4419-1478-1_14
Published:
Publisher Name: Springer, Boston, MA
Print ISBN: 978-1-4419-1477-4
Online ISBN: 978-1-4419-1478-1
eBook Packages: Chemistry and Materials ScienceChemistry and Material Science (R0)