Starting with tetracyanodibenzo(1,4,7,10-tetrathia-(12-crown-4)) (1) and 4-nitro-1,2-dicyanobenzene (2), nitro-substituted dimeric phthalocyanine (3) was synthesized. In the second step, using hydrazine hydrate as a reductant, amine-substituted dimeric phthalocyanine (4) was synthesized from nitro-substituted dimeric phthalocyanine. Structrures of all synthesized compounds were determined by elemental analyses, UV/vis, 1 H-NMR and IR spectroscopy.
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Abdurrahmanoğlu, Ş., Bulut, M., Bekaroğlu, Ö. (2009). Synthesis and Characterization of Novel Zn(II) Dimeric Phthalocyanines. In: Şener, B. (eds) Innovations in Chemical Biology. Springer, Dordrecht. https://doi.org/10.1007/978-1-4020-6955-0_42
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