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Aerobic Oxidations in Continuous Flow

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Organometallic Flow Chemistry

Part of the book series: Topics in Organometallic Chemistry ((TOPORGAN,volume 57))

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Abbreviations

Ac:

Acetyl

acac:

Acetylacetonate

ATR:

Attenuated total reflection

bpy:

2,2′-Bipyridyl

conv:

Conversion

CSTR:

Continuous stirred-tank reactor

DBU:

1,8-Diazabicyclo[5.4.0]undec-7-ene

DMF:

N,N-dimethylformamide

DMSO:

Dimethylsulfoxide

dr:

Diastereomeric ratio

equiv:

Equivalent(s)

Et:

Ethyl

EXAFS:

Extended X-ray absorption fine structure

FDH:

Formate dehydrogenase

FEP:

Fluorinated ethylene propylene

g:

Gram(s)

GC:

Gas chromatography

h:

Hour(s)

HbpA:

2-Hydroxybiphenyl 3-monooxygenase

HPLC:

High-performance liquid chromatography

IBX:

2-Iodoxybenzoic acid

i-Pr:

iso-Propyl

IR:

Infrared

L:

Liter(s)

LED:

Light-emitting diode

LOC:

Limiting oxygen concentration

m:

Meter(s)

M:

Molar

Me:

Methyl

MFC:

Mass flow controller

min:

Minute(s)

mol:

Mole(s)

MS:

Mass spectrometry

NAD:

Nicotinamide adenine dinucleotide

NaHMDS:

Sodium hexamethyldisilazide

NMI:

N-Methylimidazole

NMO:

N-Methylmorpholine N-oxide

NMP:

N-Methyl-2-pyrrolidone

n-Pr:

n-Propyl

PCC:

Pyridiniumchlorochromate

PDC:

Pyridinium dichromate

PDMS:

Polydimethylsiloxane

PEEK:

Polyether ether ketone

PEG:

Polyethylene glycol

PFA:

Perfluoroalkoxy

Ph:

Phenyl

phen:

Phenanthroline

PTFE:

Polytetrafluoroethylene

quant:

Quantitative

rt:

Room temperature

s:

Second(s)

sc:

Supercritical

Sel:

Selectivity

SET:

Single-electron transfer

SMU:

Static mixing unit

t-AmOK:

Potassium tert-amylate

TBAF:

Tetrabutylammonium fluoride

TBR:

Trickle-bed reactor

t-bu:

tert-Butyl

TEM:

Transmission electron microscopy

TEMPO:

(2,2,6,6-Tetramethylpiperidin-1-yl)oxyl

TEOS:

Tetraethoxysilane

Tf:

Trifluoromethanesulfonyl

TFA:

Trifluoroacetic acid

THF:

Tetrahydrofuran

TMEDA:

N,N,N′,N′-Tetramethyl-1,2-ethylenediamine

TMSCN:

Trimethylsilylcyanide

TPAP:

Tetrapropylammoniumperuthenate

TPP:

meso-Tetraphenylporphyrin

U:

Unit(s)

UHP:

Urea hydrogen peroxide

XAS:

X-ray absorption spectroscopy

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Acknowledgments

Research on continuous flow chemistry in our laboratories over the past decade has been generously supported by the Christian Doppler Research Association (CDG) and a variety of industrial partners including Lonza, DPx, Microinnova, ThalesNano, Anton Paar, Eli Lilly, Bayer Pharma, BASF, and Clariant.

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Authors and Affiliations

  1. Institute of Chemistry, University of Graz, NAWI Graz, Heinrichstrasse 28, 8010, Graz, Austria

    Bartholomäus Pieber & C. Oliver Kappe

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  1. Bartholomäus Pieber
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  2. C. Oliver Kappe
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Correspondence to C. Oliver Kappe .

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Editors and Affiliations

  1. Micro Flow Chemistry and Process Technology, Eindhoven University of Technology, Eindhoven, The Netherlands

    Timothy Noël

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Pieber, B., Kappe, C.O. (2015). Aerobic Oxidations in Continuous Flow. In: Noël, T. (eds) Organometallic Flow Chemistry. Topics in Organometallic Chemistry, vol 57. Springer, Cham. https://doi.org/10.1007/3418_2015_133

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