Recent Developments in Diamond-Anvil Cells

  • D. J. Dunstan
Part of the NATO ASI Series book series (ASIC, volume 401)

Abstract

Diamond-anvil cells have been simplified and miniaturised to the point where they can be added with little difficulty to a wide range of experiments. This allows high pressure, or the control of interatomic spacing, to be more generally applied in solid state physics than hitherto. The principles of the diamond-anvil cell are presented together with details of its operation in practice. Particular attention is paid to the choice and design of gasket, and to methods of pressure calibration.

Keywords

Pressure Coefficient Pressure Gauge Pressure Medium Laser Heating Uniaxial Strain 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References

  1. Adams, D.M. (1992a) High-temperature high-pressure diamond anvil cells in the Collected Abstracts of the HPG-92 IUCr Workshop on X-Ray and Neutron Diffraction at High Pressures (Washington DC, 1992).Google Scholar
  2. Adams, D.M. (1992b). See the brochures of Diacell Ltd.Google Scholar
  3. Adams, D.M., Christie, A.G. and Newman, A.J. (1992) Computer-assisted design optimization of diamond-anvil cell performance, Measurement Sci. & Tech. (to be published).Google Scholar
  4. Barnet, J.D., Block, S. and Piermarini, G.J. (1973) An optical fluorescence system for quantitative pressure measurement in the diamond-anvil cell, Rev. Sci. Instrum. 44 1–9.CrossRefGoogle Scholar
  5. Baublitz, M.A., Arnold, V. and Ruoff, A.L. (1981) Energy dispersive x-ray diffraction from high pressure polycrystalline specimens using synchroton radiation, Rev. Sci. Instrum. 52, 1616–1624.CrossRefGoogle Scholar
  6. Bell, P.M., Mao, H.K. and Goettel, K. (1984) Ultrahigh pressure: Beyond 2 megabar and the ruby fluorescence scale, Science 226 542–544.CrossRefGoogle Scholar
  7. Boehler, R. (1992) Advances in high temperature research in a diamond cel4 Proceedings of the XIII AIRAPT Conference on High Pressure Science and Technology (Bangalore, 1991) 591–600).Google Scholar
  8. Boehler, R. and Chopelas, A. (1991) A new approach to laser heating on high pressure mineral physics, Geophys. Rev. Lett. 18 1147–1150.CrossRefGoogle Scholar
  9. Burnett, J.H., Cheong, H.M. and Paul, W. (1990) The inert gases Ar, Xe and He as cryogenic pressure media, Rev. Sci. Instrum. 61 3904–3905.CrossRefGoogle Scholar
  10. Bridgman, P. (1952) The Physics of High Pressure (Bell, London).Google Scholar
  11. Dunstan, D.J. (1989) Theory of the gasket in diamond anvil high-pressure cells Rev. Sci. Instrum. 60 3789–3795.CrossRefGoogle Scholar
  12. Dunstan, D.J. and Scherer, W. (1988) Miniature diamond-anvil high-pressure cell Rev. Sci. Instrum. 59, 627–630.CrossRefGoogle Scholar
  13. Dunstan, D.J. and Spain, I.L. (1989) The technology of diamond anvil high-pressure cells: I. Principles, design and construction, J. Phys. E: Sci. Instrum. 22, 913–923.CrossRefGoogle Scholar
  14. Dunstan, D.J. and Wilkinson, V.A. (1990) Miniature cryogenic diamond anvil cell, High Pressure Research 5 794–796.CrossRefGoogle Scholar
  15. Eliseev, P.G., Sverdlov, B.N. and Shokhudzhaev, N. (1984) Reduction of the threshold current of InGaAsP/InP heterolasers by unidirectional compression, Soy. J. Quantum Electron. 14 1120–1121.CrossRefGoogle Scholar
  16. Eliseev, P.G., Sverdlov, B.N., Ismailov, I. and Shokhudzhaev, N. (1986) Influence of anisotropic deformation on the radiative characteristics of GalnAsP/InP injection lasers. I. Lasing threshold; polarisation, and watt-ampere characteristic, Soy. J. Quantum Electron. 16 1046.CrossRefGoogle Scholar
  17. Eremets, M.I., Krasnovskij, O.A., Struzhkin, V.V., Timofeev, Ju.A. and Shirokov, A.M. (1990) Method of low-temperature optical measurements with diamond anvil cells, High Pressure Research 5 880–882.CrossRefGoogle Scholar
  18. Eremets, M.I. and Shirokov, A.M. (1991) Miniature diamond anvil cells, Proceedings of the XIII AIRAPT Conference on High Pressure Science and Technology (Bangalore, 1991) 763–765.Google Scholar
  19. Eremets, M.I. and Timofeev, Ju.A. (1990) Diamond anvil microcell, Proceedings of the IV International Conference on High Pressure in Semiconductor Physics (Chalkidiki, Greece) ed. D.S. Kyriakos and O.E. Valassiades (Aristotle University, Thessaloniki, Greece), p.156.Google Scholar
  20. Grzybowski, T.A. and Ruoff, A.L. (1984) Band-overlap metallisation of BaTe, Phys. Rev. Lett. 53, 489–492.CrossRefGoogle Scholar
  21. Hemmes, H., Driessen, A., Kos, J., Mul, F.A., Griessen, R., Caro, J. and Radelaar, S., (1989) Synthesis of metal hydrides and in situ resistance measurements in a high-pressure diamond anvil cell, Rev. Sci. Instrum. 60 474–480.CrossRefGoogle Scholar
  22. Jayaraman, A. (1986) Ultrahigh pressures, Rev. Sci. Instrum. 57, 1013–1031.CrossRefGoogle Scholar
  23. Jones, G. (1992) private communication.Google Scholar
  24. Kobayashi, T. (1985) Diamond-anvil high-pressure cell for optical spectroscopy at low temperature, Rev. Sci. Instrum. 56 255–259.CrossRefGoogle Scholar
  25. Lambkin, J.D., Dunstan, D.J. and O’Reilly, E.P. (1988) The pressure dependence of the band offsets in a GalnAs/InP multiple quantum well structure, J. Crystal Growth 93, 323–328.CrossRefGoogle Scholar
  26. Leong, D., Feyrit, H., Prins, A.D., Wilkinson, V.A., Homewood, K.P. and Dunstan, D.J. (1992) Laminated gaskets for absorption and electrical measurements in the diamond anvil cell, Rev. Sci. Instrum. (in press).Google Scholar
  27. Ming, L.C. and Bassett, W.A. (1974) Laser heating in the diamond anvil press up to 2000°C sustained and 3000°C pulsed at pressures up to 260 kilobars, Rev. Sci. Instrum. 45 1115–1118.CrossRefGoogle Scholar
  28. Patel, N.B., Ripper, J.E. and Brosson, P. (1973) Behaviour of threshold current and polarisation of stimulated emission of GaAs injection lasers under uniaxial stress IEEE J. Quant. Electr. 9 338–341.CrossRefGoogle Scholar
  29. Rockwell, B., Chandrasekhar, H.R., Chandrasekhar, M., Ramdas, A.K., Kobayashi, M. and Gunshor, R.L. (1991) Pressure tuning of strains in semiconductor heterostructures: (ZnSe epilayer)l(GaAs epilayer) Phys. Rev. B44, 11307–11314.Google Scholar
  30. Ruoff, A.L. (1992) X-ray diffraction in the 500GPa range: Prospects for attaining 1TPa, Proceedings of the XIII AIRAPT Conference on High Pressure Science and Technology (Bangalore, 1991) 769–778.Google Scholar
  31. Ruoff, A.L., Luo, H. and Vohra, Y.K. (1991a) The closing diamond anvil optical window in multimegabar research, J. Appl. Phys. 69 6413–6416.CrossRefGoogle Scholar
  32. Ruoff, A.L., Luo, H., Vanderborgh, C.A. and Vohra, Y.K. (1991b) Generating near-earth-core pressures with type lia diamonds, Appl. Phys. Lett. 59 2681–2682.CrossRefGoogle Scholar
  33. Ruoff, A.L. and Vanderborgh, C.A. (1991) Hydrogen reduction of ruby at high pressure: Implications for claims of metallic hydrogen, Phys. Rev. Lett. 66 754–757.CrossRefGoogle Scholar
  34. Schroeder, W. and Webster, D.A. (1949) Press forging thin sections: Effects of friction, area and thickness on pressures required J. Appl. Mech. 16 289–294.Google Scholar
  35. Spain, I.L. and Dunstan, D.J. (1989) The technology of diamond anvil high-pressure cells: II. Operation and use, J. Phys. E: Sci. Instrum. 22, 923–933.CrossRefGoogle Scholar
  36. Sung, C.M. (1976) New modification of the diamond anvil press: A versatile apparatus for research at high pressure and high temperature, Rev. Sci. Instrum. 47, 1343–1346.CrossRefGoogle Scholar
  37. Venkateswaran, U., Chandrasekhar, H., Chandrasekhar, M., Vojak, B.A., Chambers, F.A. and Meese, J.M., (1986) High pressure studies of GaAs-Gai 4lzAs quantum wells of widths 26 to 150A, Phys. Rev. B33 8416–8423.Google Scholar
  38. Wolford, D.J., Keuch, T.F., Bradley, J.A., Gell, M.A., Nimmo, D. and Jaros, M. (1986) Pressure dependence of GaAs/Alga l B As quantum-well structures: The determination of valence-band offsets, J. Vac. Sci. Tech. B4 1043–1050.Google Scholar

Copyright information

© Springer Science+Business Media Dordrecht 1993

Authors and Affiliations

  • D. J. Dunstan
    • 1
  1. 1.Department of PhysicsUniversity of Surrey GuildfordSurreyEngland

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