Purification of Solvents

  • Heinz Engelhardt
Part of the Chemical Laboratory Practice book series (CHEMICAL LABORA)

Abstract

One of the most frequent causes of poor reproducibility in LC separations is impurities in the solvents used as eluent. Even minute traces of impurities may lead to spurious results due to their enrichment on the column, as detailed in Chapter VI. This occurs primarily during adsorption-chromatographic separations where small traces of polar contaminants, such as water, alcohol, etc. alter the properties of the system.

Keywords

Molecular Sieve Small Trace Linear Response Range Great Specific Surface Area Mixed Column 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References Chapter XII

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    Wohlleben, G.: Angew. Chem. 67, 741 (1955)CrossRefGoogle Scholar
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    Wohlleben, G.: Angew. Chem. 68, 752 (1956)CrossRefGoogle Scholar
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    Hesse, G., Schildknecht, H.: Angew. Chem. 67, 737 (1955)CrossRefGoogle Scholar
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    Hesse, G., Engelbrecht, B.P., Engelhardt, H., Nitsch, S.: Z. Anal. Chem. 241, 91 (1968)CrossRefGoogle Scholar
  5. 5.
    Engelhardt, H., in: Zief, M., Speigths, R.M. (Eds.): Ultrapurity. New York: Dekker 1972Google Scholar

Copyright information

© Springer-Verlag Berlin · Heidelberg 1979

Authors and Affiliations

  • Heinz Engelhardt
    • 1
  1. 1.Angewandte Physikalische ChemieUniversität des SaarlandesSaarbrückenGermany

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