Experimental Part

Chapter
Part of the Springer Theses book series (Springer Theses)

Abstract

All solvents were purified by distillation before use following standard procedures. Absolute solvents were obtained by distillation over appropriate drying agent (vide infra) and then kept under an atmosphere of argon: diethyl ether, tetrahydrofuran, toluene, and n-hexane (sodium, benzophenone as indicator), chloroform, dichloromethane, triethylamine (calcium hydride), ethanol (magnesium). Absolute 1,4-dioxane, TBME, di(n-butyl)ether, DME, NMP, acetonitrile, and DMSO were purchased from Sigma-Aldrich and used as received. Other commercial reagents were obtained from various sources and used without further purification.

Keywords

Nuclear Magnetic Resonance Crude Product Title Compound Combine Organic Layer Flash Column Chromatography 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Springer-Verlag Berlin Heidelberg 2012

Authors and Affiliations

  1. 1.Max-Planck-Institut für KohlenforschungMülheim an der RuhrGermany

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