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Preparation of Fe/Fe3O4 Soft Magnetic Composites by Spark Plasma Sintering

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Abstract

Fe/Fe3O4 soft magnetic composite was prepared with the method of physical coating method by spark plasma sintering. In this way, its sintering interface was improved. It solved the problem that hot pressing curing soft magnetic composites have low densification. The Fe/Fe3O4 was observed at different sintering temperatures and the influence of the chemical composition and microstructure properties was analyzed. The material density was higher and interface was combined with high performance. The resistivity decreases because the element changed with higher temperature. The morphology and structure are characterized by SEM, EDS and XRD, respectively and the electric properties are tested. In the end part we discuss the pros and cons of SPS method on synthesizing Fe/Fe3O4 soft magnetic composites and its potential application in industries.

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References

  1. J. Dong, Y. Zhang, X. Zhang, et al, Improved magnetic properties of SrFe12O19/FeCo core–shell nanofibers by hard/soft magnetic exchange–coupling effect, J. Mater. Lett. 120 (2014) 9–12.

    Google Scholar 

  2. S. Wu, A. Sun, Z. Lu, C. Cheng, X. Gao, Magnetic properties of iron-based soft magnetic composites with SiO2 coating obtained by reverse micro emulsion method, J. Magn. Mater. 381 (2015) 451–456.

    Google Scholar 

  3. Z.K. Zhao, K.F. Yao, J.F. Li, A bulk metal/ceramic composite material with a cellular structure, J. Chinese Sci. Bull. 51 (2006) 235–239.

    Google Scholar 

  4. M. Gu, H. Xu, J. Zhang, et al, Influence of hot pressing sintering temperature and time on microstructure and mechanical properties of TiB2/TiN tool material, J. Mater. Sci. Eng. 545 (2012) 1–5.

    Google Scholar 

  5. H.Y. Jin, Z.J. Ji, Y.L. Li, et al, The preparation of a core/shell structure with alumina coated spherical silica powder. Colloids and Surfaces, J. Phys. Eng. 441 (2014) 170–177.

    Google Scholar 

  6. S.R. Mishra, I. Dubenko, J. Losby, et al. Magnetic properties of magnetically soft nanocomposite Co-SiO2 prepared via mechanical milling, J. Nanosci. Nanotechno. 5 (2005) 2082–2087.

    Google Scholar 

  7. A. Khoddamzadeh, R. Liu, M. Liang et al. A new composite material - low-carbon Satellite alloy reinforced with nickel-coated carbon fibers, J. Compos. Mater. 48 (2014) 179–190.

    Google Scholar 

  8. K.J. Geng, Y.Y. Xie, L. Yan, B. Yan, Fe-Si/ZrO2 composites with core-shell structure and excellent magnetic properties prepared by mechanical milling and spark plasma sintering, J. Alloy Compos. 718 (2017) 53–62.

    Google Scholar 

  9. W.J.D. Nascimento, R.C.D. Silva, J.A. Eiras, Nanostructured Pb (Fe0.5Nb0.5)O3 ceramics obtained by spark plasma sintering, J. Integr. Ferroelectr. 174 (2016) 71–80.

    Google Scholar 

  10. Z.K. Zhao, Y.T. Sun, M.G. Wang, Y. Chi, H.L. Wang, Interfacial behavior of Fe76Si9B10P5/Zn0.5Ni0.5Fe2O4 amorphous soft magnetic composite during spark plasma sintering process. J, Sci. Mater. 26 (2016) 85–89.

    Google Scholar 

  11. R. Orru, R. Licheri, A.M. Locci, Consolidation/synthesis of materials by electric current activated/assisted sintering, J. Mater. Sci. and Eng. 63 (2009) 127–287.

    Google Scholar 

  12. K.J. Sunday, F.G. Hanejko, M.L. Taheri, Magnetic and microstructural properties of Fe3O4-coated Fe powder soft magnetic composites, J. Magn. Mater. 423 (2017) 164–170.

    Google Scholar 

  13. J. Čapek, Š. Msallamová, E. Jablonská, J. Lipovc, D. Vojtěch, A novel high-strength and highly corrosive biodegradable Fe-Pd alloy, J. Mater. Sci. Eng. 79 (2017) 550–562.

    Google Scholar 

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Correspondence to Zhankui Zhao .

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© 2018 Springer Nature Singapore Pte Ltd.

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Lu, S., Ren, J., Zhao, Z. (2018). Preparation of Fe/Fe3O4 Soft Magnetic Composites by Spark Plasma Sintering. In: Han, Y. (eds) High Performance Structural Materials. CMC 2017. Springer, Singapore. https://doi.org/10.1007/978-981-13-0104-9_7

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