Skip to main content
SpringerLink
Log in

Synthesis and Electrochemical Properties of Molybdenum Disulfide/Graphene Composites

  • Conference paper
  • First Online:
Book cover Characterization of Minerals, Metals, and Materials 2019

Part of the book series: The Minerals, Metals & Materials Series ((MMMS))

Abstract

The complex of single-layered molybdenum disulfide and graphene were widely used for capacitor field due to its better stability skeleton, higher specific surface area and conductivity. The morphology and electrochemical performance of the complex with special emphasizing effect of the amounts of graphene , volume ratio of water and ethanol in the solvent were investigated by XRD , SEM and Cyclic Voltammetry test in this work. The XRD and SEM results demonstrated that the loose flower-like spherical molybdenum disulfide could be successful synthesized at a reaction temperature of 200 °C for 24 h, a molybdenum–sulfur ratio of 1:28. And the flower-like spheroidal molybdenum disulfide was further grown on the reduced graphene oxide skeleton. It was found that the specific capacitance reached 45.4 F/g through the cyclic voltammetry test when the solvent is water. Through the AC impedance test, it was found that the addition of rGO improved the conductivity of molybdenum disulfide .

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Log in via an institution
Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 299.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Hardcover Book
USD 379.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Raghu MS, Kumar KY, Rao S et al (2018) Simple fabrication of reduced graphene oxide -few layer MoS2 nanocomposite for enhanced electrochemical performance in supercapacitors and water purification. Phys B 537:336–345

    Article  CAS  Google Scholar 

  2. Choi M, Hwang J, Setiadi H et al (2017) One-pot synthesis of molybdenum disulfide reduced graphene oxide (MoS2-RGO) composites and their high electrochemical performance as an anode in lithium ion batteries. J Supercrit Fluids 127:81–89

    Article  CAS  Google Scholar 

  3. Patil UM, Nam MS, Kang S et al (2016) Fabrication of ultra-high energy and power asymmetric supercapacitors based on hybrid 2D MoS2/graphene oxide composite electrodes: a binder-free approach. RSC Adv 6(49):43261–43271

    Article  CAS  Google Scholar 

  4. Sun T, Liu X, Li Z et al (2017) Graphene-wrapped CNT@MoS2 hierarchical structure: synthesis, characterization and electrochemical application in supercapacitors. New J Chem 41(15):7142–7150

    Article  CAS  Google Scholar 

  5. Zhuang Y-T, Zhang X, Wang D-H et al (2018) Three-dimensional molybdenum disulfide/graphene hydrogel with tunable heterointerfaces for high selective Hg(II) scavenging. J Colloid Interface Sci 514:715–722

    Article  CAS  Google Scholar 

  6. Govindasamy M, Chen SM, Mani V et al (2017) Nanocomposites composed of layered molybdenum disulfide and graphene for highly sensitive amperometric determination of methyl parathion. Microchim Acta 184(3):725–733

    Article  CAS  Google Scholar 

  7. Li X, Zhang C, Xin S et al (2016) Facile synthesis of MoS2/reduced graphene oxide@polyaniline for high-performance supercapacitors. ACS Appl Mater Interfaces 8(33):21373–21380

    Article  CAS  Google Scholar 

  8. Sun T, Li Z, Liu X et al (2016) Facile construction of 3D graphene/MoS2 composites as advanced electrode materials for supercapacitors. J Power Sources 331:180–188

    Article  CAS  Google Scholar 

  9. Bissett MA, Kinloch IA, Dryfe RAW (2015) Characterization of MoS2-graphene composites for high-performance coin cell supercapacitors. ACS Appl Mater Interfaces 7(31): 7388–17398

    Article  CAS  Google Scholar 

  10. Haitao X, Xiaopeng X (2017) A porous molybdenum disulfide and reduced graphene oxide nanocomposite (MoS2-rGO) with high adsorption capacity for fast and preferential adsorption towards Congo red. J Environ Chem Eng 5(1):1150–1158

    Google Scholar 

Download references

Acknowledgements

The authors acknowledge the financial support provided by the National Science Fund of China (No. 51674225, No. 51774252), the Innovative Talents Foundation in Universities in Henan Province (No. 18HASTIT011), the Educational Commission of Henan Province of China (No. 17A450001, 18A450001), and the China Postdoctoral Science Foundation (No. 2017M622375).

Author information

Authors and Affiliations

  1. School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou, 450001, People’s Republic of China

    Guihong Han, Wei Wang, Yanfang Huang, Yongqian Duan & Weijun Peng

  2. Henan Province Industrial Technology Research Institute of Resources and Materials, Zhengzhou University, Zhengzhou, 450001, People’s Republic of China

    Guihong Han, Wei Wang, Yanfang Huang, Yongqian Duan & Weijun Peng

Authors
  1. Guihong Han
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Wei Wang
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Yanfang Huang
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Yongqian Duan
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Weijun Peng
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding authors

Correspondence to Yanfang Huang or Weijun Peng .

Editor information

Editors and Affiliations

  1. Michigan Technological University, Houghton, MI, USA

    Bowen Li

  2. CanmetMATERIALS, Hamilton, ON, Canada

    Jian Li

  3. Al-Isra University, Amman, Jordan

    Shadia Ikhmayies

  4. ArcelorMittal Global R&D, East Chicago, IN, USA

    Mingming Zhang

  5. Middle East Technical University, Ankara, Turkey

    Yunus Eren Kalay

  6. Los Alamos National Laboratory, Los Alamos, NM, USA

    John S. Carpenter

  7. Michigan Technological University, Houghton, MI, USA

    Jiann-Yang Hwang

  8. Military Institute of Engineering, Rio de Janeiro, Brazil

    Sergio Neves Monteiro

  9. Chongqing University, Chongqing, China

    Chenguang Bai

  10. UNSW Canberra, Campbell, ACT, Australia

    Juan P. Escobedo-Diaz

  11. Free University of Bozen-Bolzano, Bolzano, Italy

    Pasquale Russo Spena

  12. Naval Research Laboratory, Washington, DC, USA

    Ramasis Goswami

Rights and permissions

Reprints and permissions

Copyright information

© 2019 The Minerals, Metals & Materials Society

About this paper

Check for updates. Verify currency and authenticity via CrossMark

Cite this paper

Han, G., Wang, W., Huang, Y., Duan, Y., Peng, W. (2019). Synthesis and Electrochemical Properties of Molybdenum Disulfide/Graphene Composites. In: Li, B., et al. Characterization of Minerals, Metals, and Materials 2019. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-05749-7_25

Download citation

Publish with us

Policies and ethics

Search

Navigation