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Nanomaterials for Liquid Chromatography and Laser Desorption/Ionization Mass Spectrometry

  • Book
  • © 2015

Overview

Authors:
  1. Tian Lu

    1. Analytical Department, Ashland Inc., Bridgewater, USA

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  • Nominated as an Outstanding Ph.D. thesis by the Ohio State University, USA
  • Highlights the application of cutting-edge nanotechnology to liquid chromatography and laser desorption/ionization mass spectrometry
  • Outlines the fundamentals, development and applications of novel nanomaterials for enhanced sensitivity, selectivity and efficiency of analyses
  • Includes supplementary material: sn.pub/extras

Part of the book series: Springer Theses (Springer Theses)

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Table of contents (7 chapters)

  1. Front Matter

    Pages i-xviii
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  2. Introduction

    • Tian Lu
    Pages 1-12

  3. Electrospun Polyvinyl Alcohol Ultra-Thin Layer Chromatography of Amino Acids

    • Tian Lu
    Pages 13-29

  4. Homogeneous Carbon as Stationary Phase for Liquid Chromatography

    • Tian Lu
    Pages 31-53

  5. Preparation of Homogeneous Basal-Plane Carbon Nanorods and Its Application for Solid Phase Extraction

    • Tian Lu
    Pages 55-63

  6. Electrospun Nanofibers as Substrates for Surface-Assisted Laser Desorption/Ionization and Matrix-Enhanced Surface-Assisted Laser Desorption/Ionization Mass Spectrometry

    • Tian Lu
    Pages 65-92

  7. Synthesis of Fluorescent Carbon

    • Tian Lu
    Pages 93-102

  8. Future Work

    • Tian Lu
    Pages 103-106

  9. Back Matter

    Pages 107-107
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Keywords

About this book

Tian Lu's dissertation describes major advances in ultrathin-layer chromatography (UTLC), liquid chromatography and surface-assisted laser desorption ionization (SALDI), and matrix-enhanced SALDI (ME-SALDI) mass spectrometry. Lu describes the fabrication of electrospun polyvinyl alcohol (PVA) UTLC plates using an in-situ crosslinking electrospinning technique. The author improved the efficiency of PVA plates greatly compared to the efficiency of silica HPTLC plates. Also highlighted in this thesis is an edge-plane based ordered-carbon surface that provides unique selectivity in liquid chromatography. Further developments include polar analytes, such as amino acids, nucleotides and nucleosides which can be well-retained and separated in the edge-plane ordered-carbon stationary phase. Also, the author studied and detected mass spectra of organic polymers as high as 900,000 Da, the highest molecular weight that has been studied by SALDI to date using the carbon nanofibrous substrate. This thesis has led to a number of publications in high-impact journals.

Authors and Affiliations

  • Analytical Department, Ashland Inc., Bridgewater, USA

    Tian Lu

Bibliographic Information

  • Book Title: Nanomaterials for Liquid Chromatography and Laser Desorption/Ionization Mass Spectrometry

  • Authors: Tian Lu

  • Series Title: Springer Theses

  • DOI: https://doi.org/10.1007/978-3-319-07749-9

  • Publisher: Springer Cham

  • eBook Packages: Chemistry and Materials Science, Chemistry and Material Science (R0)

  • Copyright Information: Springer International Publishing Switzerland 2015

  • Hardcover ISBN: 978-3-319-07748-2Published: 21 May 2015

  • Softcover ISBN: 978-3-319-36175-8Published: 09 October 2016

  • eBook ISBN: 978-3-319-07749-9Published: 07 May 2015

  • Series ISSN: 2190-5053

  • Series E-ISSN: 2190-5061

  • Edition Number: 1

  • Number of Pages: XVIII, 107

  • Number of Illustrations: 81 b/w illustrations, 16 illustrations in colour

  • Topics: Analytical Chemistry, Nanotechnology, Polymer Sciences

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