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Controlled Atmosphere Transmission Electron Microscopy

Principles and Practice

  • Thomas Willum Hansen
  • Jakob Birkedal Wagner

Table of contents

  1. Front Matter
    Pages i-viii
  2. Technique

    1. Front Matter
      Pages 1-1
    2. Ai Leen Koh, Sang Chul Lee, Robert Sinclair
      Pages 3-43
    3. Pratibha L. Gai, Edward D. Boyes, Kenta Yoshida, Thomas W. Hansen
      Pages 45-62
    4. Jakob B. Wagner, Marco Beleggia
      Pages 63-94
    5. Peter A. Crozier, Benjamin K. Miller
      Pages 95-141
    6. A. K. Erdamar, S. Malladi, F. D. Tichelaar, H. W. Zandbergen
      Pages 165-210
  3. Applications

    1. Front Matter
      Pages 211-211
    2. Jonathan Winterstein, Renu Sharma
      Pages 213-235
    3. Silvia Canepa, Sardar Bilal Alam, Duc-The Ngo, Frances M. Ross, Kristian Mølhave
      Pages 281-300
    4. Christian Jooss, Stephanie Mildner, Marco Beleggia, Daniel Mierwaldt, Vladimir Roddatis
      Pages 301-329
  4. Thomas Willum Hansen, Jakob Birkedal Wagner
    Pages E1-E2

About this book

Introduction

This book illustrates the practical workings of environmental transmission electron microscopy (ETEM) from history and instrument design through to solving practical problems. Aspects of instrument design, performance, and operating procedures are covered, together with common problems and pitfalls of the technique. Not only will a properly operated instrument and a carefully set up experiment provide new insight into your specimen, but the ability to observe the specimen in its natural habitat will be essential to meeting specific design criteria for the development of the next generation of materials. Over the past five decades, transmission electron microscopy (TEM) under environmental conditions relevant to a particular sample has been of increasing interest. Symposia dealing with the topic are now among the best attended at international microscopy conferences. Since typical operating modes for the ETEM require the sample be subjected to a harsh environment consisting of corrosive gases and high temperatures, the challenges of adapting and operating the instrument for observation under dynamic operating conditions are numerous. However, careful consideration of the interaction of the electrons with the gases and sample, as well as the gases with the microscope components, can lead to highly rewarding results. In Controlled Atmosphere Transmission Electron Microscopy, leading experts help you to perform successful experiments using the ETEM, and to interpret and understand the results.

Keywords

Catalysts and Controlled Atmosphere TEM Closed Cell Systems Controlled Atmosphere TEM Gas Handling Controlled Atmosphere TEM Instrument Controlled Atmosphere TEM Instrument Performance Controlled Atmosphere TEM, History of Controlled Atmosphere Transmission Controlled Atmostphere TEM Heating Systems ETEM Dynamic Operating Conditions ETEM Instrument Design ETEM Interpretation of Results Electron Microscopy Electron-gas-sample Effects Environmental Transmission Electron Microscopy Growth Experiments Controlled Atmosphere TEM Liquid Experiments in Controlled Atmosphere TEM Next Generation Materials TEM Book TEM Under Environmental Conditions

Editors and affiliations

  • Thomas Willum Hansen
    • 1
  • Jakob Birkedal Wagner
    • 2
  1. 1.Center for Electron NanoscopyTechnical University of DenmarkKgs. LyngbyDenmark
  2. 2.Center for Electron NanoscopyTechnical University of DenmarkKgs. LyngbyDenmark

Bibliographic information