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Journal of the Korean Physical Society

, Volume 74, Issue 2, pp 187–190 | Cite as

Use of Polyvinylpyrrolidone as a Chelating Agent to Reduce the Calcination Temperature of Li7La3Zr2O12 Synthesized by Using Solution-based Method

  • Jin-Ju Bae
  • Seon-Jin Lee
  • Jong-Tae SonEmail author
Article
  • 9 Downloads

Abstract

In general, several calcination steps and long sintering times at temperatures greater than 1000 - 1200° C are typically needed in order to achieve the more cubic structure. In this study, using polyvinylpyrrolidone as a chelating agent, cubic Li7La3Zr2O12 was synthesized at a low temperature of 900° C by using a solution-based method. The resulting cubic phase contained a small amount of the pyrochlore phase, and the lithium-ion conductivity, as determined by using electrochemical impedance spectroscopy, was 1.09 × 10−6 S/cm at 25° C.

Keywords

Li7La3Zr2O12 Reducing calcination temperature Solution-based synthesis 

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Copyright information

© The Korean Physical Society 2019

Authors and Affiliations

  1. 1.Department of Nano Polymer Science & EngineeringKorea National University of TransportationChungjuKorea

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