Skip to main content
Log in

Ellipsometric In Situ Methods of Temperature Control in the Technology of Growing MBE MCT Layers

  • Published:
Optoelectronics, Instrumentation and Data Processing Aims and scope

Abstract

The problem of in situ temperature control during the growth of epitaxial layers of HgCdTe by molecular beam epitaxy is considered. Various approaches to solving the problem using spectroscopic ellipsometry are proposed. They are based on the temperature dependence of the optical constants spectra of the CdTe buffer layer and the growing HgCdTe layer. The results of experimental testing of these methods are presented, which show that the temperature measurement accuracy is several degrees, and the sensitivity reaches fractions of a degree. At the stage of stationary growth, it is possible to determine the change not only in the temperature, but also in the composition of the growing layer from the ellipsometric spectra.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7

Similar content being viewed by others

REFERENCES

  1. J. Garland, ‘‘MBE growth of mercury cadmium telluride,’’ in Mercury Cadmium Telluride. Growth, Properties and Applications, Ed. by P. Capper and J. Garland (Wiley, 2011), pp. 131–150. https://doi.org/10.1002/9780470669464.ch7

  2. J. W. Garland and S. Sivananthan, ‘‘Molecular-beam epitaxial growth of HgCdTe,’’ in Springer Handbook of Crystal Growth, Ed. by G. Dhanaraj, K. Byrappa, V. Prasad, and M. Dudley (Springer, Berlin, 2010), pp. 1069–1132. https://doi.org/10.1007/978-3-540-74761-1_32

  3. G. L. Olson, J. A. Roth, P. D. Brewer, R. D. Rajavel, D. M. Jamba, J. E. Jensen, and B. Johs, ‘‘Integrated multi-sensor system for real-time monitoring and control of HgCdTe MBE,’’ J. Electron. Mater. 28, 749–755 (1999). https://doi.org/10.1007/s11664-999-0065-3

    Article  ADS  Google Scholar 

  4. I. V. Sabinina, A. K. Gutakovsky, Y. G. Sidorov, and A. Latyshev, ‘‘Nature of V-shaped defects in HgCdTe epilayers grown by molecular beam epitaxy,’’ J. Cryst. Growth 274, 339–346 (2005). https://doi.org/10.1016/j.jcrysgro.2004.10.053

    Article  ADS  Google Scholar 

  5. P. A. Bakhtin, V. S. Varavin, S. A. Dvoretskii, et al., ‘‘Anisotropy of conductivity of films Cd\({}_{x}\)Hg\({}_{1-x}\)Te with periodic surface microrelief grown by molecular beam epitaxy method,’’ Avtometriya 38 (2), 83–91 (2002).

    Google Scholar 

  6. I. A. Azarov, V. A. Shvets, S. A. Dulin, N. N. Mikhailov, S. S. Dvoretskii, D. G. Ikusov, I. N. Uzhakov, and S. V. Rykhlitskii, ‘‘Polarization pyrometry of layered semiconductor structures under conditions of low-temperature technological processes,’’ Optoelectron., Instrum. Data Process. 53, 630–638 (2017). https://doi.org/10.15372/AUT20170612

    Article  ADS  Google Scholar 

  7. M. Daraselia, C. H. Grein, S. Rujirawat, B. Yang, S. Sivananthan, F. Aqariden, and H. D. Shih, ‘‘In-Situ monitoring of temperature and alloy composition of Hg\({}_{1-x}\)Cd\({}_{x}\)Te using FTIR spectroscopic techniques,’’ J. Electron. Mater. 28, 743–748 (1999). https://doi.org/10.1007/s11664-999-0064-4

    Article  ADS  Google Scholar 

  8. R. Schlereth, J. Hajer, L. Fürst, S. Schreyeck, H. Buhmann, and L. W. Molenkamp, ‘‘Band edge thermometry for the MBE growth of (Hg,Cd)Te-based materials,’’ J. Cryst. Growth 537, 125602 (2020). https://doi.org/10.1016/j.jcrysgro.2020.125602

    Article  Google Scholar 

  9. L. A. Almedia, N. K. Dhar, M. Martinka, and J. H. Dinan, ‘‘HgCdTe heteroepitaxy on three-inch (112) CdZnTe/Si: Ellipsometric control of substrate temperature,’’ J. Electron. Mater. 29, 754–759 (2000). https://doi.org/10.1007/s11664-000-0220-3

    Article  ADS  Google Scholar 

  10. I. A. Azarov, D. V. Marin, V. A. Shvets, and M. V. Yakushev, ‘‘On the possibility of controlling the CdTe temperature in the MBE method using an ellipsometer,’’ in FOTONIKA 2017: Theses of Russ. Conf. on Actual Problems of Photoelectronics, Novosibirsk, 2017, P. 119.

    Google Scholar 

  11. E. V. Spesivtsev, S. V. Rykhlitskii, and V. A. Shvets, ‘‘Development of methods and instruments for optical ellipsometry at the Institute of Semiconductor Physics of the Siberian Branch of the Russian Academy of Sciences,’’ Optoelectron., Instrum. Data Process. 47, 419–425 (2011). https://doi.org/10.3103/S8756699011050219

    Article  Google Scholar 

  12. R. M. A. Azzam and N. M. Bashara, Ellipsometry and Polarized Light (North-Holland, Amsterdam, 1977).

    Google Scholar 

  13. V. A. Shvets, I. A. Azarov, D. V. Marin, M. V. Yakushev, and S. V. Rykhlitskii, ‘‘Ellipsometric method for measuring the CdTe buffer-layer temperature in the molecular-beam epitaxy of CdHgTe,’’ Semiconductors 53, 132–137 (2019). https://doi.org/10.1134/S1063782619010196

    Article  ADS  Google Scholar 

  14. D. V. Marin, V. A. Shvets, I. A. Azarov, M. V. Yakushev, and S. V. Rykhlitskii, ‘‘Ellipsometric thermometry in molecular beam epitaxy of mercury cadmium telluride,’’ Infrar. Phys. Technol. 116, 103793 (2021). https://doi.org/10.1016/j.infrared.2021.103793

    Article  Google Scholar 

  15. V. A. Shvets, D. V. Marin, V. G. Remesnik, I. A. Azarov, M. V. Yakushev, and S. V. Rykhlitskii, ‘‘Parametric model of the optical constant spectra of Hg\({}_{1-x}\)Cd\({}_{x}\)Te and determination of the compound composition,’’ Opt. Spectrosc. 128, 1948–1953 (2020). https://doi.org/10.1134/S0030400X20121042

    Article  ADS  Google Scholar 

  16. A. A. Babenko, D. V. Brunev, Yu. G. Sidorov, V. A. Shvets, and M. V. Yakushev, ‘‘Interaction of cadmium vapor with the surface of Cd\({}_{x}\)Hg\({}_{1-x}\)Te layers during molecular beam epitaxial growth on GaAs substrates,’’ Inorg. Mater. 44, 366–370 (2008). https://doi.org/10.1134/S0020168508040079

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to V. A. Shvets.

Ethics declarations

The authors declare that they have no conflicts of interest.

Additional information

Translated by E. Oborin

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Shvets, V.A., Marin, D.V., Azarov, I.A. et al. Ellipsometric In Situ Methods of Temperature Control in the Technology of Growing MBE MCT Layers. Optoelectron.Instrument.Proc. 57, 476–484 (2021). https://doi.org/10.3103/S8756699021050150

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.3103/S8756699021050150

Keywords:

Navigation