Abstract
Using the solid-phase pyrolysis and chemical vapor deposition of nickel-phthalocyanine, we have fabricated ferromagnetic Ni nanoparticles in carbon matrices. The composition, structure, morphology, and magnetic properties of samples were investigated by means of scanning electron microscopy, energy dispersive X-ray microanalysis, X-ray diffraction technique, and ferromagnetic resonance. It is shown that the sizes of nanoparticles can be varied from ∼10 nm to ∼500 nm depending on the temperature and time of pyrolysis. The used method allows us to synthesize metal nanoparticles in different carbon matrices: in amorphous carbon plates, in graphitic capsules, and in carbon nanotubes.
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Original Russian Text © A.S. Manukyan, A.A. Mirzakhanyan, G.R. Badalyan, G.H. Shirinyan, E.G. Sharoyan, 2010, published in Izvestiya NAN Armenii, Fizika, 2010, Vol. 45, No. 3, pp. 202–209.
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Manukyan, A.S., Mirzakhanyan, A.A., Badalyan, G.R. et al. Preparation and characterization of nickel nanoparticles in different carbon matrices. J. Contemp. Phys. 45, 132–136 (2010). https://doi.org/10.3103/S1068337210030060
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DOI: https://doi.org/10.3103/S1068337210030060