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Advanced experimental facilities for SHS Studies and physico-chemical characterization of inorganic materials: An autoreview

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Abstract

Overviewed are new experimental methods for investigating the processes of phase formation during SHS. The first experiments using penetrating synchrotron radiation and energy dispersive detectors for different classes of complex inorganic materials were carried out in ESRF (Grenoble, France), LURE (Orsay, France) and Daresbury (UK). A new and very sensitive thermal imaging method (Thermal Imaging Technique, TIT) is based on continuous registration of the whole combustion process by using a highly sensitive IR camera and software developed by MIKRON Instruments Co. (USA) was also used for precise registration of combustion parameters. SHS was performed on different types of pure on doped complex inorganic materials in pellet and powder form in a range of dc magnetic field induction up to 20 T and electrical field strength up to ±220 kV/m. The dc magnetic field was applied during the reaction, supplied either by permanent magnet (transverse, 1.1 T) or by an electromagnet (longitudinal, up to 20 T). The dc electrical field was applied along direction of the combustion wave propagation. The combined processes of SHS and SLS (Selective Laser Sintering) of 3D articles for different powdered compositions was realized with optimal parameters of laser irradiation, under what SHS reactions proceeded in controlled regime.

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Authors and Affiliations

  1. Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences, Cbernogolovka, Moscow, 142432, Russia

    M. V. Kuznetsov & Yu. G. Morozov

  2. Lebedev Physical Institute, Samara Branch, Russian Academy of Sciences, Samara, 43011, Russia

    I. V. Shishkovskii

Authors
  1. M. V. Kuznetsov
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  2. I. V. Shishkovskii
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  3. Yu. G. Morozov
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Correspondence to M. V. Kuznetsov.

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Kuznetsov, M.V., Shishkovskii, I.V. & Morozov, Y.G. Advanced experimental facilities for SHS Studies and physico-chemical characterization of inorganic materials: An autoreview. Int. J Self-Propag. High-Temp. Synth. 19, 191–205 (2010). https://doi.org/10.3103/S1061386210030052

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