Abstract—
A comprehensive study of the EP648 Ni-based superalloy obtained by selective laser melting followed by high-temperature annealing has been carried out. The macro- and microhardness have been studied, and the microstructure has been analyzed, while tests for brittle fracture resistance were carried out. The quantitative and qualitative analyses indicate possible structural deviations affecting the properties of products.
REFERENCES
Gibson, I., Rosen, D., and Stucker, B., Additive Production Technologies: 3D Printing, Rapid Prototyping, and Direct Digital Manufacturing, New York: Springer, 2015, 2nd ed. https://doi.org/10.1007/978-1-4939-2113-3
Petrov, I.M., Osnovnye tendentsii rossiiskogo rynka metallicheskikh poroshkov dlya additivnykh tekhnologii, Additivnye Tekhnol., 2019, no. 1, pp. 24–26.
Evgenov, A.G., Rogalev, A.M., Karachevtsev, F.N., and Mazalov, I.S., Effect of hot isostatic forming and heat treatment to properties of EP48 alloy synthesized by the method of selective laser melting, Tekhnol. Mashinostr., 2015, no. 9, pp. 11–16.
Baitimerov, R.M., Lykov, P.A., Gu, D., Zherebtcov, D.A., Nerush, S.V., and Akmedianov, A.M., Selective laser melting of nickel base heat resistance alloy EP648, Proc. Int. Conf. on Progress in Additive Manufacturing, 2016, vol. 2, pp. 445–450.
Kablov, E.N., Evgenov, A.G., Mazalov, I.S., Shurtakov, S.V., Zaytsev, D.V., and Prager, S.M., Structure and mechanical properties of alloys EP648 and VGH159 obtained by selective laser melting after simulated annealing, Materialovedenie, 2020, no. 6, pp. 3–10. https://doi.org/10.31044/1684-579X-2020-0-6-3-10
New standards in the area of additive technologies, Rosstandard, 2020. https://www.rst.gov.ru/portal/gost/home/presscenter/news.
Min, P.G., Vadeev, V.E., Rogalev, A.M., and Knyazev, A.E., The investigation of the chemical composition, structure, and mechanical properties of EP648 alloy at different stages of additive manufacturing, Inorg. Mater.: Appl. Res., 2019, vol. 10, pp. 906–911. https://doi.org/10.1134/S2075113319040257
Kablov, D.E., Sidorov, V.V., Min, P.G., and Puchkov, Yu.A., Influence of surface-active impurities and lanthanum on structure and properties of single-crystal nickel superalloy ZhS36, Tr. VIAM, 2017, no. 4, p. 2. https://doi.org/10.18577/2307-6046-2017-0-4-2-2
Products catalog, VIAM, 2022. https://catalog.viam.ru/catalog/khn50vmtyub-ep648/poroshok-iz-zharoprochnogo-nikelevogo-splava-marki-khn50vmtyub-ep648/.
GOST (State Standard) 9454-78: Metals. Method for testing the impact strength at low, room and high temperature, 1979.
Gibson, I. and Shi, D., Material properties and fabrication parameters in selective laser sintering process, Rapid Prototyping J., 1997, vol. 3, no. 4, pp. 129–136. https://doi.org/10.1108/13552549710191836
GOST (State Standard) 9450-76: Measurement of microhardness by diamond instruments indentation, 1977.
Sukhov, D.I., Mazalov, P.B., Nerush, S.V., and Khodyrev, N.A., The influence of SLS parameters on pores formation in stainless steel material, Tr. VIAM, 2017, no. 8, p. 4. https://doi.org/10.18577/2307-6046-2017-0-8-4-4
Shifeng, W., Shuai, Li, Qingsong, W., Yan, Ch., Shen, Zh., and Yusheng, Sh., Effect of molten pool boundaries on the mechanical properties of selective laser melting parts, J. Mater. Process. Technol., 2014, vol. 214, no. 11, pp. 2660–2667. https://doi.org/10.1016/j.jmatprotec.2014.06.002
Finogeev, D.Yu., Reshetnikova, O.P., Vikulova, M.A., and Pichkhidze, S.Ya., Studying the phase state of superalloy EP648 obtained by selective laser melting, Molodezh’ I XXI vek-2022. Materialy XII Mezhdunarodnoi molodezhnoi nauchnoi konferentsii (Young Scientists and 21st Century-2022: Proc. 12th Int. Young Scientists Conf.), Kursk, 2022, Razumov, M.S., Ed., Kursk: Yugo-Zapadnyi Gos. Univ., 2022, vol. 4, pp. 205–207.
Finogeev, D.Yu., Voiko, A.V, Reshetnikova, O.P., Kostin, K.B., and Pichkhidze, S.Ya., Effect of selective laser melting on structure of superalloy EP648, Perspektivy Razvitiya tekhnologii obrabotki i oborudovaniya v mashinostroenii. Sbornik nauchnykh statei 7-i Vserossiiskoi nauchno-tekhnicheskoi konferentsii s mezhdunarodnym uchastiem (Prospects of Production Technologies and Equipment in Machinery Manufacture: Proc. 7th All-Russian Sci.-Tech. Conf. with Int. Participation), Kursk, 2020, Kursk: Yugo-Zapadnyi Gos. Univ., 2022, p. 203.
Kablov, E.N., Evgenov, A.G., Ospennikova, O.G., Semenov, B.I., Semenov, A.B., and Korolev, V.A., Metal powder compositions for the EP648 superalloy manufactured by the All-Russian Research Institute for Aircraft Materials VIAM for selective laser melting, laser metal deposition and metal injection molding technologies, Izv. Vyssh. Uchebn. Zaved., Mashinostr., 2016, no. 9, pp. 62–80.
Zubchenko, A.S., Kashirskii, Yu.V., and Degtyarev, A.F., Marochnik stalei i splavov (Reference Book for Grades of Steels and Alloys), Moscow: Mashinostroenie, 2015.
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The authors are grateful to the team of Center AT (Voronezh, Russia) for their professional assistance with the sample preparation.
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Translated by N. Saetova
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Finogeev, D.Y., Reshetnikova, O.P. Effect of Heat Treatment on the Microstructure and Mechanical Properties of the EP648 Alloy Obtained by Selective Laser Melting. J. Mach. Manuf. Reliab. 52, 46–53 (2023). https://doi.org/10.3103/S1052618823010041
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DOI: https://doi.org/10.3103/S1052618823010041