Moscow University Chemistry Bulletin

, Volume 71, Issue 5–6, pp 324–328 | Cite as

Colorimetric and test determination of tetracycline and doxycycline in milk and milk products after sorption concentration at chemically modified aluminosilicate

  • E. R. Osckotskaya
  • E. N. Gribanov
  • M. N. Kalinin
  • E. V. Mitayeva
  • E. V. Panferova


A technique of colorimetric and test determination through reaction with iron(III) on the surface of chemically modified aluminosilicate for tetracycline and doxycycline was developed. The advantages of the technique are its rapidity, ease of performance, affordability, and good metrological characteristics. The method could be used in laboratories that perform chemical analysis of foodstuffs.


tetracycline doxycycline aluminosilicate colorimetry milk and milk products 


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  1. 1.
    Zolotov, Yu.A., Ivanov, V.M., and Amelin, V.G., Khimicheskie test-metody analiza (Chemical Test Methods of Analysis), Moscow: Khimiya, 2002.Google Scholar
  2. 2.
    Romanenko, G.A., Vestn. Ross. Akad. Nauk, 2004, no. 5, p. 434.Google Scholar
  3. 3.
    Aksenov, V.I. and Kovalev, V.F., Antibiotiki v produktakh zhivotnovodstva (Antibiotics in Livestock Products), Moscow: Kolos, 1977.Google Scholar
  4. 4.
    Brander, G.C., The use of antibiotics in the veterinary field in the 1970s, in Antibiotics and Antibiosis in Agriculture, Woodbin, M., Ed., London: Butterworths, 1977, p. 199.CrossRefGoogle Scholar
  5. 5.
    Melent’eva, G.A. and Antonova, L.A., Farmatsevticheskaya khimiya (Pharmaceutical Chemistry), Moscow: Meditsina, 1993.Google Scholar
  6. 6.
    Vorob’eva, T.V., in Ratsional’noe pitanie: Sb. nauch. tr. (Nutrition: Collection of Papers), Kiev, 1980, no. 15, p. 56.Google Scholar
  7. 7.
    Kal’nitskaya, O.I., Extended Abstracts of Doctoral (Vet.) Dissertation, Moscow: Russ. Acad. Agric. Sci., 2008.Google Scholar
  8. 8.
    Solovei, N.V. and Saavedra, N.F., Farmatsiya, 1974, vol. 23, no. 4, p. 72.Google Scholar
  9. 9.
    Soboleva, O.N., USSR Inventor’s Certificate no. 1081487, 1984.Google Scholar
  10. 10.
    GOST (State Standard) R 53601-2009: Food Products, Food Raw Materials. Method for Determination of the Antibiotic Residues of Tetracycline Group by High-Performance Liquid Chromatography–Mass Spectrometry (HPLC–MS), Moscow, 2011.Google Scholar
  11. 11.
    Oskotskaya, E.R., Gribanov, E.N., and Kalinin, M.N., Moscow Umiv. Chem. Bull. (Engl. Transl.), 2014, vol. 69, no. 5, p. 225.CrossRefGoogle Scholar
  12. 12.
    GOST (State Standard) R 53774-2010: Milk and Dairy Products. Immunoenzyme Methods for the Determination of Antibiotics, Moscow, 2011.Google Scholar
  13. 13.
    Kazantseva, L.K., RF Patent 2452688, 2012.Google Scholar
  14. 14.
    Lur’e, Yu.Yu., Spravochnik po analiticheskoi khimii (Handbook on Analytical Chemistry), Moscow: Khimiya, 1971.Google Scholar
  15. 15.
    Basargin, N.N., Oskotskaya, E.R., Gribanov, E.N., and Kuznetsov, E.V., J. Anal. Chem., 2012, vol. 67, no. 1, p. 35.CrossRefGoogle Scholar
  16. 16.
    Jadd, D. and Wyszecki, G., Color in Business Science and Industry, New York: Wiley, 1975.Google Scholar
  17. 17.
    Ivanov, V.M. and Kuznetsova, O.V., Russ. Chem. Rev., 2001, vol. 70, no. 5, p. 357.CrossRefGoogle Scholar
  18. 18.
    Murynov, A.I. and Khaba, B.S., Vestn. Izhevsk. Gos. Tekh. Univ., 2002, no. 3, p. 96.Google Scholar

Copyright information

© Allerton Press, Inc. 2016

Authors and Affiliations

  • E. R. Osckotskaya
    • 1
  • E. N. Gribanov
    • 1
  • M. N. Kalinin
    • 1
  • E. V. Mitayeva
    • 1
  • E. V. Panferova
    • 1
  1. 1.Orel State UniversityOrelRussia

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