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Colorimetric and test determination of tetracycline and doxycycline in milk and milk products after sorption concentration at chemically modified aluminosilicate

Moscow University Chemistry Bulletin Aims and scope

Abstract

A technique of colorimetric and test determination through reaction with iron(III) on the surface of chemically modified aluminosilicate for tetracycline and doxycycline was developed. The advantages of the technique are its rapidity, ease of performance, affordability, and good metrological characteristics. The method could be used in laboratories that perform chemical analysis of foodstuffs.

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References

  1. Zolotov, Yu.A., Ivanov, V.M., and Amelin, V.G., Khimicheskie test-metody analiza (Chemical Test Methods of Analysis), Moscow: Khimiya, 2002.

    Google Scholar 

  2. Romanenko, G.A., Vestn. Ross. Akad. Nauk, 2004, no. 5, p. 434.

    Google Scholar 

  3. Aksenov, V.I. and Kovalev, V.F., Antibiotiki v produktakh zhivotnovodstva (Antibiotics in Livestock Products), Moscow: Kolos, 1977.

    Google Scholar 

  4. Brander, G.C., The use of antibiotics in the veterinary field in the 1970s, in Antibiotics and Antibiosis in Agriculture, Woodbin, M., Ed., London: Butterworths, 1977, p. 199.

    Chapter  Google Scholar 

  5. Melent’eva, G.A. and Antonova, L.A., Farmatsevticheskaya khimiya (Pharmaceutical Chemistry), Moscow: Meditsina, 1993.

    Google Scholar 

  6. Vorob’eva, T.V., in Ratsional’noe pitanie: Sb. nauch. tr. (Nutrition: Collection of Papers), Kiev, 1980, no. 15, p. 56.

    Google Scholar 

  7. Kal’nitskaya, O.I., Extended Abstracts of Doctoral (Vet.) Dissertation, Moscow: Russ. Acad. Agric. Sci., 2008.

    Google Scholar 

  8. Solovei, N.V. and Saavedra, N.F., Farmatsiya, 1974, vol. 23, no. 4, p. 72.

    CAS  Google Scholar 

  9. Soboleva, O.N., USSR Inventor’s Certificate no. 1081487, 1984.

    Google Scholar 

  10. GOST (State Standard) R 53601-2009: Food Products, Food Raw Materials. Method for Determination of the Antibiotic Residues of Tetracycline Group by High-Performance Liquid Chromatography–Mass Spectrometry (HPLC–MS), Moscow, 2011.

  11. Oskotskaya, E.R., Gribanov, E.N., and Kalinin, M.N., Moscow Umiv. Chem. Bull. (Engl. Transl.), 2014, vol. 69, no. 5, p. 225.

    Article  Google Scholar 

  12. GOST (State Standard) R 53774-2010: Milk and Dairy Products. Immunoenzyme Methods for the Determination of Antibiotics, Moscow, 2011.

  13. Kazantseva, L.K., RF Patent 2452688, 2012.

    Google Scholar 

  14. Lur’e, Yu.Yu., Spravochnik po analiticheskoi khimii (Handbook on Analytical Chemistry), Moscow: Khimiya, 1971.

    Google Scholar 

  15. Basargin, N.N., Oskotskaya, E.R., Gribanov, E.N., and Kuznetsov, E.V., J. Anal. Chem., 2012, vol. 67, no. 1, p. 35.

    Article  CAS  Google Scholar 

  16. Jadd, D. and Wyszecki, G., Color in Business Science and Industry, New York: Wiley, 1975.

    Google Scholar 

  17. Ivanov, V.M. and Kuznetsova, O.V., Russ. Chem. Rev., 2001, vol. 70, no. 5, p. 357.

    Article  CAS  Google Scholar 

  18. Murynov, A.I. and Khaba, B.S., Vestn. Izhevsk. Gos. Tekh. Univ., 2002, no. 3, p. 96.

    Google Scholar 

Download references

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Correspondence to E. R. Osckotskaya.

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Original Russian Text © E.R. Osckotskaya, E.N. Gribanov, M.N. Kalinin, E.V. Mitayeva, E.V. Panferova, 2016, published in Vestnik Moskovskogo Universiteta, Seriya 2: Khimiya, 2016, No. 5, pp. 350–355.

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Osckotskaya, E.R., Gribanov, E.N., Kalinin, M.N. et al. Colorimetric and test determination of tetracycline and doxycycline in milk and milk products after sorption concentration at chemically modified aluminosilicate. Moscow Univ. Chem. Bull. 71, 324–328 (2016). https://doi.org/10.3103/S0027131416050060

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  • DOI: https://doi.org/10.3103/S0027131416050060

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