Abstract
A technique of colorimetric and test determination through reaction with iron(III) on the surface of chemically modified aluminosilicate for tetracycline and doxycycline was developed. The advantages of the technique are its rapidity, ease of performance, affordability, and good metrological characteristics. The method could be used in laboratories that perform chemical analysis of foodstuffs.
References
Zolotov, Yu.A., Ivanov, V.M., and Amelin, V.G., Khimicheskie test-metody analiza (Chemical Test Methods of Analysis), Moscow: Khimiya, 2002.
Romanenko, G.A., Vestn. Ross. Akad. Nauk, 2004, no. 5, p. 434.
Aksenov, V.I. and Kovalev, V.F., Antibiotiki v produktakh zhivotnovodstva (Antibiotics in Livestock Products), Moscow: Kolos, 1977.
Brander, G.C., The use of antibiotics in the veterinary field in the 1970s, in Antibiotics and Antibiosis in Agriculture, Woodbin, M., Ed., London: Butterworths, 1977, p. 199.
Melent’eva, G.A. and Antonova, L.A., Farmatsevticheskaya khimiya (Pharmaceutical Chemistry), Moscow: Meditsina, 1993.
Vorob’eva, T.V., in Ratsional’noe pitanie: Sb. nauch. tr. (Nutrition: Collection of Papers), Kiev, 1980, no. 15, p. 56.
Kal’nitskaya, O.I., Extended Abstracts of Doctoral (Vet.) Dissertation, Moscow: Russ. Acad. Agric. Sci., 2008.
Solovei, N.V. and Saavedra, N.F., Farmatsiya, 1974, vol. 23, no. 4, p. 72.
Soboleva, O.N., USSR Inventor’s Certificate no. 1081487, 1984.
GOST (State Standard) R 53601-2009: Food Products, Food Raw Materials. Method for Determination of the Antibiotic Residues of Tetracycline Group by High-Performance Liquid Chromatography–Mass Spectrometry (HPLC–MS), Moscow, 2011.
Oskotskaya, E.R., Gribanov, E.N., and Kalinin, M.N., Moscow Umiv. Chem. Bull. (Engl. Transl.), 2014, vol. 69, no. 5, p. 225.
GOST (State Standard) R 53774-2010: Milk and Dairy Products. Immunoenzyme Methods for the Determination of Antibiotics, Moscow, 2011.
Kazantseva, L.K., RF Patent 2452688, 2012.
Lur’e, Yu.Yu., Spravochnik po analiticheskoi khimii (Handbook on Analytical Chemistry), Moscow: Khimiya, 1971.
Basargin, N.N., Oskotskaya, E.R., Gribanov, E.N., and Kuznetsov, E.V., J. Anal. Chem., 2012, vol. 67, no. 1, p. 35.
Jadd, D. and Wyszecki, G., Color in Business Science and Industry, New York: Wiley, 1975.
Ivanov, V.M. and Kuznetsova, O.V., Russ. Chem. Rev., 2001, vol. 70, no. 5, p. 357.
Murynov, A.I. and Khaba, B.S., Vestn. Izhevsk. Gos. Tekh. Univ., 2002, no. 3, p. 96.
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © E.R. Osckotskaya, E.N. Gribanov, M.N. Kalinin, E.V. Mitayeva, E.V. Panferova, 2016, published in Vestnik Moskovskogo Universiteta, Seriya 2: Khimiya, 2016, No. 5, pp. 350–355.
About this article
Cite this article
Osckotskaya, E.R., Gribanov, E.N., Kalinin, M.N. et al. Colorimetric and test determination of tetracycline and doxycycline in milk and milk products after sorption concentration at chemically modified aluminosilicate. Moscow Univ. Chem. Bull. 71, 324–328 (2016). https://doi.org/10.3103/S0027131416050060
Received:
Published:
Issue Date:
DOI: https://doi.org/10.3103/S0027131416050060