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Extraction and subsequent determination of dialkyl phthalates in the soil using gas chromatography combined with tandem mass spectrometry

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Moscow University Chemistry Bulletin Aims and scope

Abstract

A method for the extraction and subsequent quantitative determination of dialkyl phthalates (DAPs) in soil using gas chromatography combined with tandem mass spectrometry is suggested. The method is characterized by low limits of detection, as well as high sensitivity and selectivity. The optimal conditions for DAP extraction from soils were selected and evaluation of the possible secondary contamination of DAP samples from labware and chemicals and distribution of DAP in soil were performed.

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Authors and Affiliations

  1. Department of Chemistry, Moscow State University, Moscow, Russia

    A. V. Pirogov, N. G. Tolmacheva & O. A. Shpigun

Authors
  1. A. V. Pirogov
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  2. N. G. Tolmacheva
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  3. O. A. Shpigun
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Corresponding author

Correspondence to N. G. Tolmacheva.

Additional information

Original Russian Text © A.V. Pirogov, N.G. Tolmacheva, O.A. Shpigun, 2014, published in Vestnik Moskovskogo Universiteta. Khimiya, 2014, No. 4, pp. 207–213.

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Pirogov, A.V., Tolmacheva, N.G. & Shpigun, O.A. Extraction and subsequent determination of dialkyl phthalates in the soil using gas chromatography combined with tandem mass spectrometry. Moscow Univ. Chem. Bull. 69, 158–162 (2014). https://doi.org/10.3103/S0027131414040087

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  • DOI: https://doi.org/10.3103/S0027131414040087

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