Abstract
The concentration of metal ions(Cd2 * Cu2+ Pb2+ Mn2+ Zn2* and Fe3+) on 1-phenyl-3-methyl-4-stearoy1-5-pyrazo-lone(Cl8) loaded on silica gel(Cl8/SG) was investigated by batch and column methods. At pH values higher than 6, these metals were quantitatively retained on C18/SG. The adsorbent did not change its retention efficiency for the metals for at least 6 adsorption/elution cycles. Results of determinations of these metals in environmental samples were satisfactory.
Similar content being viewed by others
References
M. A. Marshall, H. A. Mottla, Anal. Chem., 55, 2089 (1983)
K. Oshima, H. Watanabe, K. Haragucni, Anal. Sci., 2, 131 (1986)
D. E. Leyden, G. H. Lutrell, Anal. Chem., 47, 1612 (1975)
T. Seshadri, A. Kettrup, Fresenius' Z. Anal. Chem., 296, 247 (1979)
A. Tong, Y. Akama, S. Tanaka, Anal. Chim. Acta, 230, 179 (1990)
K. Terada, K. Morimoto and T. Kiba, Anal. Chim. Acta, 116, 127 (1980)
K. Terada, K. Nakamura, Talanta, 28, 123 (1981)
A. Tong, Y. Akama and S. Tanaka, Analyst, 115, 947 (1990)
A. Tong, Y. Akama and S. Tanaka, Anal. Chim. Acta, 230, 175 (1990)
K. Sato, Y. Akama and T. Nakai, Anal. Chim. Acta, 207, 367 (1988)
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Tong, A., Akama, Y. Preconcentration of Trace Metals with 1-Phenyl-3-Methyl-4-Stearoyl-5-Pyrazolone Loaded on Silica Gel. ANAL. SCI. 7 (Suppl 1), 83–86 (1991). https://doi.org/10.2116/analsci.7.Supple_83
Published:
Issue Date:
DOI: https://doi.org/10.2116/analsci.7.Supple_83