Abstract
An anion-exchange chromatographic method has been developed for simultaneous analysis of cyanuric acid (CA) and five inorganic anions (F-, Cl-, NO3-, HPO42- and SO42-) in milk powder. The separation was achieved within 15 min on an anion-exchange column with simple elution of Na2CO3/NaHCO3 buffer as mobile phase. Furthermore, the effect of the total concentration of Na2CO3/NaHCO3 buffer on the retention of five inorganic anions was more obvious than that on CA retention, which indicated that CA retention on anion-exchange column depends not only on anion-exchange interaction but also on hydrophobic interactions between CA and anion-exchange column. The linear range of the calibration curve for CA was 0.1 - 100 mg L-1. The detection limit calculated at S/N = 3 was 0.083 mg L-1. The method was successfully applied to the analysis of CA in milk powder.
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References
R. Cantu, O. Evans, F. K. Kawahara, J. A. Shoemaker, and A. P. Dufour, Anal. Chem., 2000, 72, 5820.
A. Kirk, “Encyclopedia of Chemical Technology”, 1993, John Wiley & Sons, New York, 834 - 851.
C. Yu, L. Zhu, J. Xiao, H. Tang, G. Guo, Q. Zeng, and X. Wang, Food Control, 2009, 20, 205.
C. A. Brown, K. S. Jeong, R. H. Poppenga, B. Puschner, D. M. Miller, and A. E. Ellis, J. Vet. Diagn. Invest., 2007, 19, 525.
B. Puschner, R. H. Poppenga, L. J. Lowenstine, M. S. Filigenzi, and P. A. Pesavento, J. Vet. Diagn. Invest., 2007, 19, 616.
Y. C. Fiamegos, C. N. Konidari, and C. D. Stalikas, Anal. Chem., 2003, 75, 4034.
H. Miao, S. Fan, Y Wu, L. Zhang, P. Zhou, J. Li, H. Chen, and Y Zhao, Biomed. Environ. Sci., 2009, 22, 87.
R. Cantú, O. Evans, F. K. Kawahara, L. J. Wymer, and A. P. Dufour, Anal. Chem., 2001, 73, 3358.
K. Patel and K. Jones, J. Chromatogr, B, 2007, 853, 360.
M. L. Magnuson, C. A. Kelty, and R. J. Am Cantú, Soc. Mass. Spectrom., 2001, 12, 1085.
A Desmarchelier, M. G. Cuadra, T. Delatour, and P. J. Mottier, J. Agric. Food Chem., 2009, 57, 7186.
M. S. Filigenzi, B. Puschner, L. S. Aston, and R. H. Poppenga, J. Agric. Food Chem., 2008, 56, 7593.
B. N. Tran, R. Okoniewski, R. Storm, R. Jansing, and K. M. Aldous, J. Agric. Food Chem., 2010, 58, 101.
E. Pelizzeti, V. Maurino, C. Minero, V. Carlin, E. Pramauro, O. Zerbinati, and M. L. Tosato, Environ. Sci. Technol., 1990, 24, 1559.
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Wang, H., Hou, S., Ding, M. et al. Determination of Cyanuric Acid in Milk Powder by Anion-exchange Chromatography. ANAL. SCI. 26, 1305–1308 (2010). https://doi.org/10.2116/analsci.26.1305
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DOI: https://doi.org/10.2116/analsci.26.1305