Skip to main content
Log in

A Fast, Simple Calibration Method for Organic Carbon Isotope Analysis Using Continuous-flow Elemental Analyzer Interfaced with an Isotope Ratio Mass Spectrometer

  • Notes
  • Published:
Analytical Sciences Aims and scope Submit manuscript

Abstract

Continuous flow analysis using an elemental analyzer interfaced with an isotope ratio mass spectrometer (EA-IRMS) is faster and requires much less material than conventional analytical methods. Although using an EA-IRMS is simple and fast, accurate calibration strongly depends on matching sample and reference peak heights by adjusting the sample weight. This paper describes a new modification for calibration using only the major ion beam intensity (nA) without weighing each sample or increasing the number of reference materials.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. D. J. Croft and K. Pye, Rapid Commun. Mass Spectrom., 2003, 17, 2581.

    Article  CAS  Google Scholar 

  2. T. Preston and N. J. P. Owens, Analyst, 1983, 108, 971.

    Article  CAS  Google Scholar 

  3. T. Preston and N. J. P. Owens, Biomed. Mass Spectrom., 1985, 12, 510.

    Article  CAS  Google Scholar 

  4. K. E. A. Ohlsson and P. H. Wallmark, Analyst, 1999, 124, 571.

    Article  Google Scholar 

  5. N. V. Grassineau, Appl. Geochem., 2006, 21, 756.

    Article  CAS  Google Scholar 

  6. GV Instruments, Application Note, 507.

  7. GV Instruments, IsoPrime EA Training Manual, 2005.

  8. J. Morrison, T. Brockwell, T. Merren, F. Fourel, and A. M. Phillips, Anal. Chem., 2001, 73, 3570.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Kwang-Sik Lee.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Bong, YS., Lee, KS. A Fast, Simple Calibration Method for Organic Carbon Isotope Analysis Using Continuous-flow Elemental Analyzer Interfaced with an Isotope Ratio Mass Spectrometer. ANAL. SCI. 23, 1447–1449 (2007). https://doi.org/10.2116/analsci.23.1447

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.2116/analsci.23.1447

Navigation