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Simultaneous Determination of Sodium Dialkyldithiocarbamates by Ion Exchange Chromatography

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Abstract

A simple and reliable method is described for the determination of sodium dialkyldithiocarbamates (R2NCS2Na: R=CH3, C2H5, n-C3H7, and n-C4H9) by high performance liquid chromatography. They were injected onto a column packed with the strongly basic anion exchanger and separated with an eluent of acetonitrile-phosphate buffer containing no ion-pairing reagent. This method was applied to the analysis of commercially available R2NCS2Na. It was demonstrated that the results are in good agreement with those obtained by the Potentiometric titration.

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Authors and Affiliations

  1. Department of Pharmaceutical Sciences, Setsunan University, Nagao-Toge, Hirakata, 573-01, Japan

    Tadahiro Tetsumi & Masao Sumi

  2. Department of Applied Chemistry, Faculty of Engineering, Osaka University, Yamadaoka, Suita, 565, Japan

    Minoru Tanaka & Toshiyuki Shono

Authors
  1. Tadahiro Tetsumi
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  2. Masao Sumi
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  3. Minoru Tanaka
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  4. Toshiyuki Shono
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Tetsumi, T., Sumi, M., Tanaka, M. et al. Simultaneous Determination of Sodium Dialkyldithiocarbamates by Ion Exchange Chromatography. ANAL. SCI. 2, 77–80 (1986). https://doi.org/10.2116/analsci.2.77

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  • DOI: https://doi.org/10.2116/analsci.2.77

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