Skip to main content
Log in

Setting evaluation of cement mortar using nondestructive methods under different curing conditions: temperatures and relative humidities

  • Original Article
  • Published:
Materials and Structures Aims and scope Submit manuscript

Abstract

In this study, the effects of the curing conditions on the setting of cement mortars are investigated using nondestructive methods, electrical resistivity and ultrasonic wave velocity. Nine curing cases with different temperatures and relative humidities were considered. The electrical resistivity and ultrasonic wave velocity were monitored for 24 h after mixing to evaluate the setting and hardening. In addition, mercury intrusion porosimetry was combined with X-ray diffraction analysis to explore the differences in the results between the two nondestructive methods. The obtained nondestructive parameters from the electrical resistivity and ultrasonic wave velocity measurements showed different trends according to the changed curing conditions. High relative humidity at constant temperature induced carbonation of calcium hydroxide more than at low relative humidity, resulting in pore refinement by the calcium carbonate precipitation. The carbonation during the curing process did not affect the solid-phase network in ultrasonic wave velocity, while the electrical resistivity was affected by the pore water due to the carbonation.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10

Similar content being viewed by others

References

  1. Mehta PK, Monteiro PJM (2006) Concrete: microstructure, properties, and materials. McGraw-Hill, New York

    Google Scholar 

  2. Tao Y, Rahul AV, Lesage K et al (2021) Stiffening control of cement-based materials using accelerators in inline mixing processes: possibilities and challenges. Cem Concr Compos 119:103972. https://doi.org/10.1016/j.cemconcomp.2021.103972

    Article  Google Scholar 

  3. Loukili A, Chopin D, Khelidj A, Le Touzo J-Y (2000) A new approach to determine autogenous shrinkage of mortar at an early age considering temperature history. Cem Concr Res 30:915–922. https://doi.org/10.1016/S0008-8846(00)00241-6

    Article  Google Scholar 

  4. Jiang C, Yang Y, Wang Y et al (2014) Autogenous shrinkage of high performance concrete containing mineral admixtures under different curing temperatures. Constr Build Mater 61:260–269. https://doi.org/10.1016/j.conbuildmat.2014.03.023

    Article  Google Scholar 

  5. Ramezanianpour AA, Malhotra VM (1995) Effect of curing on the compressive strength, resistance to chloride-ion penetration and porosity of concretes incorporating slag, fly ash or silica fume. Cem Concr Compos 17:125–133. https://doi.org/10.1016/0958-9465(95)00005-W

    Article  Google Scholar 

  6. (2008) ASTM C191-08, Standard Test Methods for Time of Setting of Hydraulic Cement by Vicat Needle. ASTM Int West Conshohocken, PA, USA

  7. (2008) ASTM C403-08, Standard Test Methods for Time of Setting of Concrete Mixtures by Penetration Resistance. ASTM Int West Conshohocken, PA, USA

  8. Yim HJ, Bae YH, Jun Y (2021) Hydration and microstructural characterization of early-age cement paste with ultrasonic wave velocity and electrical resistivity measurements. Constr Build Mater 303:124508. https://doi.org/10.1016/j.conbuildmat.2021.124508

    Article  Google Scholar 

  9. Ylmén R, Jäglid U, Steenari B-M, Panas I (2009) Early hydration and setting of Portland cement monitored by IR, SEM and Vicat techniques. Cem Concr Res 39:433–439. https://doi.org/10.1016/j.cemconres.2009.01.017

    Article  Google Scholar 

  10. Langan BW, Weng K, Ward MA (2002) Effect of silica fume and fly ash on heat of hydration of Portland cement. Cem Concr Res 32:1045–1051. https://doi.org/10.1016/S0008-8846(02)00742-1

    Article  Google Scholar 

  11. Akkaya Y, Voigt T, Subramaniam KV, Shah SP (2003) Nondestructive measurement of concrete strength gain by an ultrasonic wave reflection method. Mater Struct 36:507–514. https://doi.org/10.1007/BF02480827

    Article  Google Scholar 

  12. Voigt T, Grosse CU, Sun Z et al (2005) Comparison of ultrasonic wave transmission and reflection measurements with P- and S-waves on early age mortar and concrete. Mater Struct 38:729–738. https://doi.org/10.1007/BF02479285

    Article  Google Scholar 

  13. Estévez E, Martín DA, Argiz C, Sanjuán MÁ (2020) Ultrasonic pulse velocity—compressive strength relationship for Portland cement mortars cured at different conditions. Curr Comput-Aided Drug Des 10:133

    Google Scholar 

  14. Xiao L, Li Z (2008) Early-age hydration of fresh concrete monitored by non-contact electrical resistivity measurement. Cem Concr Res 38:312–319. https://doi.org/10.1016/j.cemconres.2007.09.027

    Article  Google Scholar 

  15. Bentz DP (2007) Cement hydration: building bridges and dams at the microstructure level. Mater Struct 40:397–404. https://doi.org/10.1617/s11527-006-9147-3

    Article  Google Scholar 

  16. Xiao L, Li Z, Wei X (2007) Selection of superplasticizer in concrete mix design by measuring the early electrical resistivities of pastes. Cem Concr Compos 29:350–356. https://doi.org/10.1016/j.cemconcomp.2006.12.015

    Article  Google Scholar 

  17. Schwarz N, DuBois M, Neithalath N (2007) Electrical conductivity based characterization of plain and coarse glass powder modified cement pastes. Cem Concr Compos 29:656–666. https://doi.org/10.1016/j.cemconcomp.2007.05.005

    Article  Google Scholar 

  18. Yim HJ, Lee H, Kim JH (2017) Evaluation of mortar setting time by using electrical resistivity measurements. Constr Build Mater 146:679–686. https://doi.org/10.1016/j.conbuildmat.2017.04.088

    Article  Google Scholar 

  19. Zhang W, Zhang Y, Liu L et al (2012) Investigation of the influence of curing temperature and silica fume content on setting and hardening process of the blended cement paste by an improved ultrasonic apparatus. Constr Build Mater 33:32–40. https://doi.org/10.1016/j.conbuildmat.2012.01.011

    Article  Google Scholar 

  20. Yim HJ, Kim JH, Shah SP (2014) Ultrasonic monitoring of the setting of cement-based materials: frequency dependence. Constr Build Mater 65:518–525. https://doi.org/10.1016/j.conbuildmat.2014.04.128

    Article  Google Scholar 

  21. Trtnik G, Turk G, Kavčič F, Bosiljkov VB (2008) Possibilities of using the ultrasonic wave transmission method to estimate initial setting time of cement paste. Cem Concr Res 38:1336–1342. https://doi.org/10.1016/j.cemconres.2008.08.003

    Article  Google Scholar 

  22. Topçu İB, Uygunoğlu T, Hocaoğlu İ (2012) Electrical conductivity of setting cement paste with different mineral admixtures. Constr Build Mater 28:414–420. https://doi.org/10.1016/j.conbuildmat.2011.08.068

    Article  Google Scholar 

  23. (2006) KS L ISO 679, Methods of Testing Cements-Determination of Strength. Korean Stand Assoc

  24. (2001) ASTM G57, Standard Test Method for Field Measurement of Soil Resistivity Using the Wenner Four-Electrode Method. ASTM Int West Conshohocken, PA, USA

  25. Zhang J, Scherer GW (2011) Comparison of methods for arresting hydration of cement. Cem Concr Res 41:1024–1036. https://doi.org/10.1016/j.cemconres.2011.06.003

    Article  Google Scholar 

  26. Belsky A, Hellenbrandt M, Karen VL, Luksch P (2002) New developments in the Inorganic Crystal Structure Database (ICSD): accessibility in support of materials research and design. Acta Crystallogr Sect B 58:364–369

    Article  Google Scholar 

  27. (2007) PDF-2 Database Sets, International Centre for Diffraction Data

  28. Robeyst N, Grosse CU, De Belie N (2009) Measuring the change in ultrasonic p-wave energy transmitted in fresh mortar with additives to monitor the setting. Cem Concr Res 39:868–875. https://doi.org/10.1016/j.cemconres.2009.06.016

    Article  Google Scholar 

  29. Kjellsen KO, Detwiler RJ (1992) Reaction kinetics of portland cement mortars hydrated at different temperatures. Cem Concr Res 22:112–120. https://doi.org/10.1016/0008-8846(92)90141-H

    Article  Google Scholar 

  30. Lv Q, Ren Z, Xiao L (2019) Study on temperature effect of hydration behavior of cement pastes. IOP Conf Ser Mater Sci Eng 562:12084. https://doi.org/10.1088/1757-899x/562/1/012084

    Article  Google Scholar 

  31. Berodier E, Bizzozero J, Muller ACA (2015) Chapter 9: Mercury intrusion porosimetry. In: Scrivener K, Snellings R, Lothenbach B (eds) A practical guide to microstructural analysis of cementitious materials. Taylor & Francis Group

  32. Fernández Á, García Calvo JL, Alonso MC (2018) Ordinary Portland cement composition for the optimization of the synergies of supplementary cementitious materials of ternary binders in hydration processes. Cem Concr Compos 89:238–250. https://doi.org/10.1016/j.cemconcomp.2017.12.016

    Article  Google Scholar 

  33. Zhang Q, Ye G (2012) Dehydration kinetics of Portland cement paste at high temperature. J Therm Anal Calorim 110:153–158. https://doi.org/10.1007/s10973-012-2303-9

    Article  Google Scholar 

  34. Tavakoli D, Tarighat A (2016) Molecular dynamics study on the mechanical properties of Portland cement clinker phases. Comput Mater Sci 119:65–73. https://doi.org/10.1016/j.commatsci.2016.03.043

    Article  Google Scholar 

  35. Kim MS, Jun Y, Lee C, Oh JE (2013) Use of CaO as an activator for producing a price-competitive non-cement structural binder using ground granulated blast furnace slag. Cem Concr Res 54:208–214. https://doi.org/10.1016/j.cemconres.2013.09.011

    Article  Google Scholar 

  36. Alarcon-Ruiz L, Platret G, Massieu E, Ehrlacher A (2005) The use of thermal analysis in assessing the effect of temperature on a cement paste. Cem Concr Res 35:609–613. https://doi.org/10.1016/j.cemconres.2004.06.015

    Article  Google Scholar 

  37. Chan C-M, Wu J, Li J-X, Cheung Y-K (2002) Polypropylene/calcium carbonate nanocomposites. Polymer (Guildf) 43:2981–2992. https://doi.org/10.1016/S0032-3861(02)00120-9

    Article  Google Scholar 

  38. Fares H, Remond S, Noumowe A, Cousture A (2010) High temperature behaviour of self-consolidating concrete: microstructure and physicochemical properties. Cem Concr Res 40:488–496. https://doi.org/10.1016/j.cemconres.2009.10.006

    Article  Google Scholar 

  39. Cazalla O, Rodriguez-Navarro C, Sebastian E et al (2000) Aging of lime putty: effects on traditional lime mortar carbonation. J Am Ceram Soc 83:1070–1076. https://doi.org/10.1111/j.1151-2916.2000.tb01332.x

    Article  Google Scholar 

  40. Ashraf W, Olek J (2018) Carbonation activated binders from pure calcium silicates: reaction kinetics and performance controlling factors. Cem Concr Compos 93:85–98. https://doi.org/10.1016/j.cemconcomp.2018.07.004

    Article  Google Scholar 

Download references

Funding

This work was supported by the National Research Foundation of Korea (NRF) Grant funded by the Korea government (MSIT) (No. NRF-2022R1C1C1009589).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Hong Jae Yim.

Ethics declarations

Conflict of interest

The authors declare no conflict of interest.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Jun, Y., Bae, Y.H. & Yim, H.J. Setting evaluation of cement mortar using nondestructive methods under different curing conditions: temperatures and relative humidities. Mater Struct 56, 43 (2023). https://doi.org/10.1617/s11527-023-02138-4

Download citation

  • Received:

  • Accepted:

  • Published:

  • DOI: https://doi.org/10.1617/s11527-023-02138-4

Keywords

Navigation