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Evaluation of Si3N4/AISI 304 steel joints produced by reactive brazing using Cu–Zn filler alloy

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Abstract

The objective of this work is focused in the accomplishment of Si3N4/Cu–Zn/AISI 304 joints and its interfacial study during liquid-state bonding. Sandwich type assemblies Si3N4/Cu–Zn/AISI 304 were produced at temperatures of 950 °C, 980 °C, and 1000 °C using different holding times (1–40 min) in argon atmosphere. The interfaces were characterized through SEM using EPMA in order to reveal the interaction between contact surfaces during joining process. The results showed that Si3N4 could not be bonded to AISI 304 at temperature lower than 1000 °C; however, successful joining was achieved at 1000 °C. Joining occurred by the formation of a reactive interface with several reaction products on the metal side of the joint. Shear testing gave a maximum joint strength of 66 MPa for Si3N4/Cu–Zn/AISI 304 samples produced at 1000 °C and 15 min, showing the intimate relationship between the interface and the joint strength.

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Acknowledgements

The authors would like to thank to Universidad Michoacana de San Nicolás de Hidalgo (UMSNH) and CONACYT Mexico for the facilities of this research.

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Authors and Affiliations

  1. Instituto de Investigación en Metalurgia y Materiales, Universidad Michoacana de San Nicolás de Hidalgo, Fco. J. Mújica S/N, Edif. U, C.U., Apdo. Postal 888, C.P. 58000, Morelia, Mich., Mexico

    Ángel del Jesús León-Gerónimo, Quetzalmaflor Miranda-Hernández, Jorge A. Verduzco-Martínez & José Lemus-Ruiz

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  1. Ángel del Jesús León-Gerónimo
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  2. Quetzalmaflor Miranda-Hernández
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  3. Jorge A. Verduzco-Martínez
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Correspondence to José Lemus-Ruiz.

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The authors declare that the datasets generated during and/or analyzed during the current study are included in full in the results of this paper.

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León-Gerónimo, Á., Miranda-Hernández, Q., Verduzco-Martínez, J.A. et al. Evaluation of Si3N4/AISI 304 steel joints produced by reactive brazing using Cu–Zn filler alloy. MRS Advances 6, 932–936 (2021). https://doi.org/10.1557/s43580-021-00183-1

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