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Synchronous microwave and ultrasound irradiation for the synthesis of SBA-15

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Abstract

Green chemistry is today the most important methodology to develop and improve processes for obtaining mesoporous materials. SBA-15 is a siliceous mesoporous material with a hexagonal structure. In this work, SBA-15-type material was synthesized by the Sol–Gel method and subsequently irradiated by microwave, ultrasound, and synchronous irradiation (microwave/ultrasound) in the aging stage. The synthesized materials using microwave/ultrasound irradiation showed similar characteristics to the SBA-15 material synthesized by the Sol–Gel method, with marked differences for each heat treatment. Furthermore, the sample obtained by synchronous irradiation showed the best textural properties by combining microwave and ultrasound irradiation. It improves the synthesis time, reducing it to one minute in the aging stage.

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Acknowledgments

We gratefully acknowledge the CONACyT-Mexico postdoctoral fellowship awarded to FDVH.

Funding

The authors did not receive support from any organization for the submitted work.

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Authors and Affiliations

  1. Laboratorio de Nanomateriales Sustentables, Escuela Superior de Ingeniería Química e Industrias Extractivas, Instituto Politécnico Nacional, Ed Z-5 2do Piso, UPALM Zacatenco, 07738, Mexico City, Mexico

    Josue Flores-Cantera & Silvia Patricia Paredes-Carrera

  2. Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla, Av. San Claudio, Ciudad Universitaria, 72570, Puebla, PUE, Mexico

    Jorge Alejandro Cruz-Mérida

  3. Laboratorio de Materiales Bioactivos, Facultad de Ciencias Químicas, Benemérita Universidad Autónoma de Puebla, Av. San Claudio, Ciudad Universitaria, 72570, Puebla, PUE, Mexico

    Franchescoli Didier Velázquez-Herrera

  4. Unidad Académica Profesional Acolman, Universidad Autónoma del Estado de México, Camino de Caleros #11, Ejidos de Santa Catarina, 55875, Acolman, Estado de México, Mexico

    Yohuali Zarazua-Aguilar

Authors
  1. Josue Flores-Cantera
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  2. Jorge Alejandro Cruz-Mérida
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  3. Franchescoli Didier Velázquez-Herrera
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  4. Silvia Patricia Paredes-Carrera
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  5. Yohuali Zarazua-Aguilar
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Correspondence to Yohuali Zarazua-Aguilar.

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Flores-Cantera, J., Cruz-Mérida, J.A., Velázquez-Herrera, F.D. et al. Synchronous microwave and ultrasound irradiation for the synthesis of SBA-15. MRS Communications 12, 388–393 (2022). https://doi.org/10.1557/s43579-022-00190-9

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  • DOI: https://doi.org/10.1557/s43579-022-00190-9

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