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Substrate and film structure impacts on adhesion properties between lignocellulosic polymers

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Abstract

Using AFM, ellipsometric and profilometric measurements, we have investigated the topography and the thickness of the cellulose nanocristal (NCC) films prepared by two different methods: the first one is obtained by evaporation of concentrated suspension of NCC in petri-dish to produce a self-supported film; the second one is produced by dipping thin NCC layer on silicon substrate by Langmuir-Blodgett (LB) technique. Glucomanan (GM) functionalized AFM tip was brought into contact with these two kinds of NCC films in order to measure the adhesion between GM and NCC. The impact of the substrate and the thickness of NCC films on the measured adhesion forces were also studied: the mean measured adhesion force between the two polysaccharides was 17 nN regardless of the way the films were prepared. Adhesion properties can help us understand biochemical processes in the plant cell wall.

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Acknowledgments

This work was partly finantially supported by ANR-08-BLAN-0009 “Analogs” and Champagne-Ardennes Region program NANOBIO2.

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Authors and Affiliations

  1. Laboratoire de Microscopie et d’Etude de Nanostructure, Université de Reims Champagne-Ardenne, F-51100, Reims, France

    Elias Estephan, Loïc Muraille & Michael Molinari

  2. INRA, UMR 614 Fractionnement des AgroRessources et Environnement, F-51100, Reims, France

    Elias Estephan, Véronique Aguié-Béghin & Loïc Muraille

  3. UMR 614, Fractionnement des AgroRessources et Environnement, Université Reims Champagne-Ardennes, F-51100, Reims, France

    Elias Estephan, Véronique Aguié-Béghin & Loïc Muraille

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  1. Elias Estephan
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  2. Véronique Aguié-Béghin
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  3. Loïc Muraille
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  4. Michael Molinari
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Estephan, E., Aguié-Béghin, V., Muraille, L. et al. Substrate and film structure impacts on adhesion properties between lignocellulosic polymers. MRS Online Proceedings Library 1422, 1–6 (2012). https://doi.org/10.1557/opl.2012.55

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  • DOI: https://doi.org/10.1557/opl.2012.55

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