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Analysis of Complex Microstructures: Serial Sectioning and Phase-Field Simulations

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Abstract

With the emergence and evolution of serial sectioning techniques that allow for three-dimensional data collection and the continuing increase in computational power, it is now possible to analyze and compute the evolution of three-dimensional nano- and microstructures. Structures can be accurately characterized, and it is possible to correlate processing paths with materials properties with great precision. Examples of the analysis and computations of the evolution of three-dimensional microstructures are discussed. The focus is on experiments that use serial sectioning methods to determine three-dimensional structure and on phase-field simulations of microstructural evolution that employ experimental three-dimensional data as initial conditions.

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References

  1. R.T. DeHoff, J. Microsc. 131, 259 (1983).

    Google Scholar 

  2. D. Basanta, M.A. Miodownik, E.A. Holm, P.J. Bentley, Metall. Mater. Trans. A 36A, 1643 (2005).

    Google Scholar 

  3. P. Kenesei, H. Biermann, A. Borbély, Scripta Mater. 53, 787 (2005).

    Google Scholar 

  4. A. Borbély, P. Kenesei, H. Biermann, Acta Mater. 54, 2735 (2006).

    Google Scholar 

  5. T.F. Bower, H.D. Brody, M.C. Flemings, Trans. AIME 236, 624 (1966).

    Google Scholar 

  6. M.A. Mangan, P.D. Lauren, G.J. Shiflet, J. Met. 188, 36 (1997).

    Google Scholar 

  7. M. Li, S. Ghosh, O. Richmond, H. Weiland, T.N. Rouns, Mater. Sci. Eng. A265, 153 (1999).

    Google Scholar 

  8. M. Li, S. Ghosh, O. Richmond, H. Weiland, T.N. Rouns, Mater. Sci. Eng. A266, 221 (1999).

    Google Scholar 

  9. R.T. DeHoff, E.H. Aigeltinger, K.R. Craig, J. Microsc. 95, 69 (1972).

    Google Scholar 

  10. J. Alkemper, P.W. Voorhees, J. Microsc. 201, 388 (2001).

    Google Scholar 

  11. J.E. Spowart, H.M. Mullens, B.T. Puchala, J. Met. 55, 35 (2003).

    Google Scholar 

  12. A.C. Lewis, J.F. Bingert, D.J. Rowenhorst, A. Gupta, A.B. Geltmacher, G. Spanos, Mater. Sci. Eng. 418, 11 (2006).

    Google Scholar 

  13. D.J. Rowenhorst, A. Gupta, C.R. Feng, G. Spanos, Scripta Mater. 55, 11 (2006).

    Google Scholar 

  14. M.D. Uchic, M.A. Groeber, D.M. Dimiduk, J.P. Simmons, Scripta Mater. 55, 23 (2006).

    Google Scholar 

  15. M. Groeber, S. Ghosh, M.D. Uchic, D.M. Dimiduk, J. Met. 59, 32 (2007).

    Google Scholar 

  16. J.R. Wilson, W. Kobsiriphat, R. Mendoza, Hsun-Yi Chen, J.M. Miller, D.J. Miller, K. Thornton, P.W. Voorhees, S.B. Adler, S.A. Barnett, Nat. Mater. 5, 541 (2006).

    Google Scholar 

  17. L. Holzer, F. Indutnyi, P.H. Gasser, B. Muench, M. Wegmann, J. Microsc. 216, 84 (2004).

    Google Scholar 

  18. L. Holzer, B. Muench, M. Wegmann, P. Gasser, R.J. Flatt, J. Am. Ceram. Soc. 89, 2577 (2006).

    Google Scholar 

  19. D. Bernard, O. Nielsen, L. Salvo, P. Cloetens, Mater. Sci. Eng. A 392, 112 (2005).

    Google Scholar 

  20. O. Ludwig. M. Dimichiel, L. Salvo, M. Suéry, P. Falus, Metall. Mater. Trans. A 36A, 1515 (2005).

    Google Scholar 

  21. N. Limodin, L. Salvo, M. Suéry, M. Dimichiel, Acta Mater. 55, 3177 (2007).

    Google Scholar 

  22. D. Isheim, R. Prakash Kolli, M.E. Fine, D.N. Seidman, Scripta Mater. 55, 35 (2006).

    Google Scholar 

  23. E.M. Lauridsen, S. Schmidt, S.F. Nielsen, L. Margulies, H.F. Poulsen, D. Juul Jensen, Scripta Mater. 55, 51 (2006).

    Google Scholar 

  24. E. Maire, P. Colombo, J. Adrien, L. Babout, L. Biasetto, J. Eur. Ceram. Soc. 27, 1973 (2007).

    Google Scholar 

  25. H.M. Singer, J.H. Bilgram, Europhys. Lett. 68, 240 (2004).

    Google Scholar 

  26. W.E. Lorensen, H.E. Cline, Comput. Graphics 21, 163 (1987).

    Google Scholar 

  27. M. Gameiro, K. Mischaikow, T. Wanner, Acta Mater. 53, 693 (2005).

    Google Scholar 

  28. D. Kammer, PhD Thesis, Northwestern University, Evanston, IL, June 2006.

  29. J. Alkemper, P.W. Voorhees, Acta Mater. 49, 897 (2001).

    Google Scholar 

  30. J. Alkemper, R. Mendoza, P.W. Voorhees, Adv. Eng. Mater. 4, 694 (2002).

    Google Scholar 

  31. R. Mendoza, J. Alkemper, P.W. Voorhees, Metall. Mater. Trans. A 34A, 481 (2003).

    Google Scholar 

  32. R. Mendoza, J. Alkemper, P.W. Voorhees, Z. Metallkd. 96, 155 (2005).

    Google Scholar 

  33. D. Kammer, P.W. Voorhees, Acta Mater. 54, 1549 (2006).

    Google Scholar 

  34. R. Mendoza, K. Thornton, I. Savin, P.W. Voorhees, Acta Mater. 54, 743 (2006).

    Google Scholar 

  35. D. Kammer, R. Mendoza, P.W. Voorhees, Scripta Mater. 55, 17 (2006).

    Google Scholar 

  36. T.L. Wolfsdorf, W.H. Bender, P.W. Voorhees, Acta Mater. 45, 2279 (1997).

    Google Scholar 

  37. D.J. Rowenhorst, J.P. Kuang, K. Thornton, P.W. Voorhees, Acta Mater. 54, 2027 (2006).

    Google Scholar 

  38. H. Jinnai, T. Koga, Y. Nishikawa, T. Hashimoto, S. Hyde, Phys. Rev. Lett. 78, 2248 (1997).

    Google Scholar 

  39. Y. Nishikawa, H. Jinnai, T. Koga, T. Hasimoto, S. Hyde, Langmuir 14, 1242 (1998).

    Google Scholar 

  40. Y. Nishikawa, T. Koga, T. Hashimoto, H. Jinnai, Langmuir 17, 3254 (2001).

    Google Scholar 

  41. J.E. Spowart, Scripta Mater. 55, 5 (2006).

    Google Scholar 

  42. B. Maruyama, J.E. Spowart, D.J. Hooper, H.M. Mullens, A.M. Druma, C. Druma, M. Khairul Alam, Scripta Mater. 54 (2006).

  43. J.E. Spowart, J. Met. 58, 29 (2006).

    Google Scholar 

  44. J.W. Gibbs, The Collected Works of J. Williard Gibbs (Oxford University Press, Oxford, UK, 1948).

    Google Scholar 

  45. J.D. van der Waals, Z. Phys. Chem. 13, 657 (1894).

    Google Scholar 

  46. W.J. Boettinger, J.A. Warren, C. Beckermann, A. Karma, Annu. Rev. Mater. Res. 32, 163 (2002).

    Google Scholar 

  47. M. Ode, S.G. Kim, T. Suzuki, ISIJ Int. 41, 1076 (2001).

    Google Scholar 

  48. L.Q. Chen, Annu. Rev. Mater. Res. 32, 113 (2002).

    Google Scholar 

  49. G. Caginalp, W. Xie, Phys. Rev. E 48, 1897 (1993).

    Google Scholar 

  50. A.A. Wheeler, W.J. Boettinger, G.B. McFadden, Phys. Rev. A 45, 7424 (1992).

    Google Scholar 

  51. A. Karma, W.J. Rappel, Phys. Rev. E 53, 3017 (1996).

    Google Scholar 

  52. P.W. Bates, P.C. Fife. R.A. Gardner, C.K.R.T. Jones, Phys. D 104, 1 (1997).

    Google Scholar 

  53. N. Provatas, N. Goldenfeld, J. Dantzig, J. Comp. Phys. 148, 265 (1999).

    Google Scholar 

  54. N. Provatas, N. Goldenfeld, J. Dantzig, Phys. Rev. Lett. 80, 3308 (1998).

    Google Scholar 

  55. J. Gruber, N. Ma, Y. Wang, A.D. Rollett, G.S. Rohrer, Modell. Simul. Mater. Sci. Eng. 14, 1189 (2006).

    Google Scholar 

  56. R. Mendoza, I. Savin, K. Thornton, P.W. Voorhees, Nat. Mater. 3, 385 (2004).

    Google Scholar 

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Kammer, D., Voorhees, P.W. Analysis of Complex Microstructures: Serial Sectioning and Phase-Field Simulations. MRS Bulletin 33, 603–610 (2008). https://doi.org/10.1557/mrs2008.125

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