Abstract
In this study, Aluminum-based nanocomposites with hybrid reinforcements were successfully prepared by mechanical alloying, followed by consolidation using selective laser melting (SLM). The evolution of particle morphology and microstructural features of the milled powders at various milling times was studied. The results indicated that the milled powder particles experienced a coarsening stage at the early 5 h milling and followed by a continuous refinement during 5–20 h milling. After 20 h of milling, the original coarse needle-like Al3.21Si0.47 evolved into nanometer/submicrometer-sized spherical Al3.21Si0.47. Meanwhile, both fine Al3.21Si0.47 and ex-situ nanoscale TiN particles distributed uniformly within the Al matrix. By SLM processing of the 20-h powder, a near fully dense part with a uniform microstructure consisting of circularly dispersed and submicrometer-sized reinforcement particles embedded in α-Al matrix was obtained. The Vickers hardness and coefficient of friction of the SLM-processed part reached 178 HV0.1 and 0.38, respectively.
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P.H.C. Camargo, K.G. Satyanarayana, and F. Wypych: Nanocomposites: Synthesis, structure, properties and new application opportunities. Mater. Res. 12(1), 1 (2009).
T. Sekino and K. Niihara: Microstructural characteristics and mechanical properties for Al2O3/metal nanocomposites. Nanostruct. Mater. 6(5), 663 (1995).
S. Seal, S.C. Kuiry, R. Georgieva, and A. Agarwal: Manufacturing nanocomposite parts: Present status and future challenges. MRS Bull. 29(1), 16 (2004).
D.L. Zhang: Processing of advanced materials using high-energy mechanical milling. Prog. Mater. Sci. 49(3), 537 (2004).
S. Hwang and C. Nishimnra: Compressive mechanical properties of Mg–Ti–C nanocomposite synthesized by mechanical milling. Scr. Mater. 44(10), 2457 (2001).
G. Marta, D. Jan, and M. Jerzy: Effect of reinforcement particle size on microstructure and mechanical properties of AlZnMgCu/AlN nano-composites produced using mechanical alloying. J. Alloys Compd. 586(1), S423 (2014).
M.H. Enayati and F.A. Mohamed: Application of mechanical alloying/milling for synthesis of nanocrystalline and amorphous materials. Int. Mater. Rev. 59(7), 394 (2014).
D.S. Zhou, D.L. Zhang, C. Kong, P. Munroe, and R. Torrens: Thermal stability of the nanostructure of mechanically milled Cu-5 vol% Al2O3 nanocomposite powder particles. J. Mater. Res. 29(8), 996 (2014).
M.S. El-Eskandarany: Mechanical solid state mixing for synthesizing of SiCp/Al nanocomposites. J. Alloys Compd. 279(2), 263 (1998).
G.Q. Zhang and D.D. Gu: Synthesis of nanocrystalline TiC reinforced W nanocomposites by high-energy mechanical alloying: Microstructural evolution and its mechanism. Appl. Surf. Sci. 273, 364 (2013).
J.P. Kruth, P. Mercelis, J.V. Vaerenbergh, L. Froyen, and M. Rombouts: Binding mechanisms in selective laser sintering and selective laser melting. Rapid Prototyping J. 11(1), 26 (2005).
H. Attar, M. Bönisch, M. Calin, L.C. Zhang, K. Zhuravleva, A. Funk, S. Scudino, C. Yang, and J. Eckert: Comparative study of microstructures and mechanical properties of in situ Ti–TiB composites produced by selective laser melting, powder metallurgy, and casting technologies. J. Mater. Res. 29(17), 1941 (2014).
D.D. Gu, W. Meiners, K. Wissenbach, and R. Poprawe: Laser additive manufacturing of metallic components: Materials, processes and mechanisms. Int. Mater. Rev. 53(3), 133 (2012).
E.O. Olakanmi, R.F. Cochrane, and K.W. Dalgarno: A review on selective laser sintering/melting (SLS/SLM) of aluminium alloy powders: Processing, microstructure, and properties. Prog. Mater. Sci. 74, 401 (2015).
B. Vrancken, L. Thijs, J.P. Kruth, and J.V. Humbeeck: Microstructure and mechanical properties of a novel β titanium metallic composite by selective laser melting. Acta Mater. 68(15), 150 (2014).
H.Q. Wang and D.D. Gu: Nanometric TiC reinforced AlSi10Mg nanocomposites: Powder preparation by high-energy ball milling and consolidation by selective laser melting. J. Compos. Mater. 0, 1 (2014).
Z.M. Li, D. Chen, H.W. Wang, E.J. Lavernia, and A.D. Shan: Nano-TiB2 reinforced ultrafine-grained pure Al produced by flux-assisted synthesis and asymmetrical rolling. J. Mater. Res. 29(21), 2514 (2014).
K.D. Woo and D.L. Zhang: Fabrication of Al–7wt%Si–0.4wt%Mg/SiC nanocomposite powders and bulk nanocomposites by high energy ball milling and powder metallurgy. Curr. Appl. Phys. 4(2), 175 (2004).
L. Jiang, H.M. Wen, H.R. Yang, T. Hu, T. Topping, D.L. Zhang, E.J. Lavernia, and J.M. Schoenung: Influence of length-scales on spatial distribution and interfacial characteristics of B4C in a nanostructured Al matrix. Acta Mater. 89, 327 (2015).
D. Poirier, R. Gauvin, and R.A.L. Drew: Characterization of the fabrication steps of a CNTs-al nanocomposite. Microsc. Microanal. 13, 668 (2007).
E. Mohammad Sharifi and F. Karimzadeh: Wear behavior of aluminum matrix hybrid nanocomposites fabricated by powder metallurgy. Wear 271, 1072 (2011).
C. Suryanarayana: Mechanical alloying and milling. Prog. Mater. Sci. 46(1), 1 (2001).
I. Yamauchi, K. Takahara, T. Tanaka, and K. Matsubara: Chemical leaching of rapidly solidified Al–Si binary alloys. J. Alloys Compd. 396(1), 302 (2005).
E. Karakose and M. Keskin: Effect of solidification rate on the microstructure and microhardness of a melt-spun Al–8Si–1Sb alloy. J. Alloys Compd. 476(1), 230 (2009).
X.X. Dong, L.J. He, and G.B. Mi: Two directional microstructure and effects of nanoscale dispersed Si particles on microhardness and tensile properties of AlSi7Mg melt-spun alloy. J. Alloys Compd. 618, 609 (2015).
A. Bendijk, R. Delhez, L. Katgerman, T.H. De Keijser, E.J. Mittemeijer, and N.M. Van Der Pers: Characterization of Al–Si-alloys rapidly quenched from the melt. J. Mater. Sci. 15(11), 2803 (1980).
E.J. Mittemeijer: Fundamentals of Materials Science, 1st ed. (Springer-Verlag Berlin Heidelberg, Berlin, 2010); p. 154.
C.R. Clark, C. Suryanarayana, and F.H. Froes: Advances in Powder Metallurgy and Particulate Materials-1995: Part 1 (Metal Powder Industries Federation, Princeton, NJ, 1995); pp. 135–145.
X. Wu, N. Tao, Y. Hong, B. Xu, J. Lu, and K. Lu: Microstructure and evolution of mechanically-induced ultrafine grain in surface layer of AL-alloy subjected to USSP. Acta Mater. 50(8), 2075 (2002).
N.R. Tao, Z.B. Wang, W.P. Tong, M.L. Sui, J. Lu, and K. Lu: An investigation of surface nanocrystallization mechanism in Fe induced by surface mechanical attrition treatment. Acta Mater. 50(18), 4603 (2002).
M. Wen, G. Liu, J.F. Gu, W.M. Guan, and J. Lu: Dislocation evolution in titanium during surface severe plastic deformation. Appl. Surf. Sci. 255(12), 6097 (2009).
J.B. Fogagnolo, F. Velasco, M.H. Robert, and J.M. Torralba: Effect of mechanical alloying on the morphology, microstructure and properties of aluminum matrix composite powders. Mater. Sci. Eng., A 342(1), 131 (2003).
S.B. Sun, L.J. Zheng, Y.Y. Liu, J.H. Liu, and H. Zhang: Characterization of Al–Fe–V–Si heat-resistant aluminum alloy components fabricated by selective laser melting. J. Mater. Res. 30(10), 1661 (2015).
J.P. Kruth, G. Levy, F. Klocke, and T.H.C. Childs: Consolidation phenomena in laser and powder-bed based layered manufacturing. CIRP Ann. Manuf. Technol. 56(2), 730 (2007).
D.D. Gu: Laser Additive Manufacturing of High-Performance Materials (Springer-Verlag Berlin Heidelberg, Berlin, 2015); pp. 175–198.
D. Buchbinder, H. Schleifenbaum, S. Heidrich, W. Meiners, and J. Bultmann: High power selective laser melting (HP SLM) of aluminum parts. Phys. Proc. 12, 271 (2011).
ACKNOWLEDGMENTS
We appreciate the financial support from the National Natural Science Foundation of China (No. 51322509), the Outstanding Youth Foundation of Jiangsu Province of China (No. BK20130035), the Program for New Century Excellent Talents in University (No. NCET-13-0854), the Science and Technology Support Program (The Industrial Part), Jiangsu Provincial Department of Science and Technology of China (No. BE2014009-2), and the Fundamental Research Funds for the Central Universities (Nos. NE2013103 and NP2015206).
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Ma, C., Gu, D., Dai, D. et al. Aluminum-based nanocomposites with hybrid reinforcements prepared by mechanical alloying and selective laser melting consolidation. Journal of Materials Research 30, 2816–2828 (2015). https://doi.org/10.1557/jmr.2015.267
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DOI: https://doi.org/10.1557/jmr.2015.267