Abstract
The effect of electric-current pulses on the evolution of microstructure and texture in cryogenically rolled copper was determined. The pulsed material was found to be completely recrystallized, and the recrystallization mechanism was deduced to be similar to that operating during conventional static annealing. The microstructural changes were explained simply in terms of Joule heating. A significant portion of the recrystallization process was concluded to have occurred after pulsing; i.e., during cooling to ambient temperature. The grain structure and microhardness were shown to vary noticeably in the heat-affected zone (HAZ); these observations mirrored variations of temper colors. Accordingly, the revealed microstructure heterogeneity was attributed to the inhomogeneous temperature distribution developed during pulsing. In the central part of the HAZ, the mean grain size increased with current density and this effect was associated with the temperature rise per se. This grain size was slightly smaller than that in statically recrystallized specimens.
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ACKNOWLEDGMENTS
The authors thank Dr. R.M. Galeyev and Dr. O.R. Valiakhmetov for graciously providing the material used in this work, and P. Klassman and T.I. Nazarova for technical assistance during cryogenic rolling. One of the authors (AVK) would like to acknowledge the Tomsk State University Competitiveness Improvement Program for financial support.
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Konkova, T., Valeev, I., Mironov, S. et al. Effect of electric-current pulses on grain-structure evolution in cryogenically rolled copper. Journal of Materials Research 29, 2727–2737 (2014). https://doi.org/10.1557/jmr.2014.299
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DOI: https://doi.org/10.1557/jmr.2014.299