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Error estimation of nanoindentation mechanical properties near a dissimilar interface via finite element analysis and analytical solution methods

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Abstract

Nanoindentation methods are well suited for probing the mechanical properties of a heterogeneous surface, since the probe size and contact volumes are small and localized. However, the nanoindentation method may introduce errors in the computed mechanical properties when indenting near the interface between two materials having significantly different mechanical properties. Here we examine the case where a soft material is loaded in close proximity to an interface of higher modulus, such as the case when indenting bone near a metallic implant. The results are derived from both an approximate analytical quarter space solution and a finite element model, and used to estimate the error in indentation-determined elastic modulus as a function of the distance from the apex of contact to the dissimilar interface, for both Berkovich and spherical indenter geometries. Sample data reveal the potential errors in mechanical property determination that can occur when indenting near an interface having higher stiffness, or when characterizing strongly heterogeneous materials. The results suggest that caution should be used when interpreting results in the near-interfacial region.

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References

  1. R.B. King: Elastic analysis of some punch problems for a layered medium. Int. J. Solids Struct. 23, 1657 (1987)

    Google Scholar 

  2. W.C. Oliver and G.M. Pharr: An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7, 1564 (1992).

    CAS  Google Scholar 

  3. J.S. Field and M.V. Swain: A simple predictive model for spherical indentation. J. Mater. Res. 8, 297 (1993).

    CAS  Google Scholar 

  4. S.V. Hainsworth, H.W. Chandler, and T.F. Page: Analysis of nanoindentation load displacement loading curves. J. Mater. Res. 11, 1987 (1996).

    CAS  Google Scholar 

  5. Y.T. Cheng and C.M. Cheng: What is indentation hardness? Surf. Coat. Technol. 417, 133 (2000).

    CAS  Google Scholar 

  6. S.G. Lewis, J. Beumer, G.R. Perri, and W.P. Hornburg: Single tooth implant supported restorations. Int. J. Oral Maxil. Imp. 3, 25 (1988).

    CAS  Google Scholar 

  7. T. Jemt: Modified single and short-span restorations supported by osseointegrated fixtures in the partially edentulous jaw. J. Prosthet. Dent. 55, 243 (1986).

    CAS  Google Scholar 

  8. P.T. Branemark, R. Adell, T. Albrektsson, U. Lekholm, S. Lundkvist, and B. Rockier: Osseointegrated titanium fixtures in the treatment of edentulousness. Biomaterials 4, 25 (1983).

    CAS  Google Scholar 

  9. M.C. Chang, C.C. Ko, C.C. Liu, W.H. Douglas, R. DeLong, W-J. Seong, J. Hodges, and K-N. An: Elasticity of alveolar bone near dental implant-bone interfaces after one month’s healing. J. Biomech. 36, 1209 (2003).

    CAS  Google Scholar 

  10. P.A. Clark, A.M. Clark, A. Rodriguez, M.A. Hussain, and J.J. Mao: Nanoscale characterization of bone-implant interface and biome-chanical modulation of bone ingrowth. Mater. Sci. Ens.. C 27, 382 (2007).

    CAS  Google Scholar 

  11. H. Graf: Occlusal forces during function, in Proceedings of Symposium on Occlusion: Research on Form and Function, edited by A. Rowe (University of Michigan School of Dentistry, Ann Arbor, MI, 1975), p. 90.

    Google Scholar 

  12. H.Y. Chou, J.J. Jagodnik, and S. Muftu: Predictions of bone remodeling around dental implant systems. J. Biomech. 41, 1365 (2008).

    Google Scholar 

  13. S.C. Cowin: Bone stress adaptation models. J. Biomech. Ens. 115, 528 (1993).

    CAS  Google Scholar 

  14. J.E. Jakes, C.R. Frihart, J.F. Beecher, R.J. Moon, and D.S. Stone: Experimental method to account for structural compliance in nanoindentation measurements. J. Mater. Res. 23, 1113 (2008).

    CAS  Google Scholar 

  15. Ya.S. Uflyand: Second basic problem of elasticity for a wedge. Trudy Leningr. Politekh. In-ta. 210, 87 (1960).

    Google Scholar 

  16. Ya.S. Uflyand: Some spatial elasticity problems for a wedge, in Continuum Mechanics and Related Problems of Analysis (Nauka, Moscow, 1972), p. 549.

    Google Scholar 

  17. J. Shim, H. Nakamura, and T. Ogawa: An understanding of the mechanism that promotes adhesion between roughened titanium implants and mineralized tissue. J. Biomech. Ens. 131, 054503 (2009).

    Google Scholar 

  18. G.Ya. Popov: An exact solution of the mixed elasticity problem in a quarter-space. Mech. Solids 38, 23 (2003).

    Google Scholar 

  19. H. Hertz: On the contact of elastic solids. J. Reine Angew. Math 92, 156 (1881).

    Google Scholar 

  20. A. Fischer-Cripps: Nanoindentation (Springer, New York, 2002).

    Google Scholar 

  21. G.M. Pharr, W.C. Oliver, and F.R. Brotzen: On the generality of the relationship among contact stiffness, contact area, and the elastic modulus during indentation. J. Mater. Res. 7, 613 (1992).

    CAS  Google Scholar 

  22. A.E.H. Love: Boussinesq’s problem for a rigid cone. O. J. Math. 10, 161 (1939)

    Google Scholar 

  23. J. Zhang, G.L. Niebur, and T.C. Ovaert: Mechanical property determination of bone through nano- and micro-indentation testing and finite element simulation. J. Biomech. 41, 267 (2008).

    Google Scholar 

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Correspondence to T. C. Ovaert.

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Zhao, Y., Ovaert, T.C. Error estimation of nanoindentation mechanical properties near a dissimilar interface via finite element analysis and analytical solution methods. Journal of Materials Research 25, 2308–2316 (2010). https://doi.org/10.1557/jmr.2010.0295

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  • DOI: https://doi.org/10.1557/jmr.2010.0295

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