Abstract
Dislocations have been imaged in bulk specimens of Si using a FEG SEM operating at 30keV and 100keV, without using an energy filter, but by image processing of the back scattered electron signal collected by a highly efficient detector. The dislocation contrast is greater at 30 keV than at 10OkeV. Ilowever, the depth to which useful information may be obtained is greater at 1O0keV (∼210nm) than at 3OkeV (∼95nm). The final depth to which dislocations can be imaged is strongly dependent on image processing conditions.
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References
- [1]
P. Morin, M. Pitaval, D. Besnard and G. Fontaine, Phil. Mag., 40, 511 (1979).
- [2]
J.T. Czcrnuszka, N.J. Long, E.D. Boyes and P.B. Hirsch, Phil. Mag. Letts. 62,227 (1990).
- [3]
J.T. Czernuszka, N.J. Long and P. B. Hirsch, in Proc. XIIth International Congress on Electron Microscopy Vol. 4 p.410 (1990).
- [4]
D.R. Clarke and A. Howie, Phil. Mag. 24, 259 (1971).
- [5]
J.P. Spencer, C.J. Humphreys and P.B. Hirsch, Phil. Mag., 26193 (1972).
- [6]
G. Fontaine, P. Morin, and M. Pitaval, Inst. Phvs. Conf. Ser. no.67: section 4, p. pp{213} (1987)
Acknowledgement
SERC are thanked for funding and for a Research Fellowship to one of us (JTC). T.Fell prepared the silicon sample and J. Stead helped with the construction of the detector.
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Czernuszka, J.T., Long, N.J., Boyes, E.D. et al. Electron Channelling Contrast Imaging (ECCI) of Dislocations in Bulk Specimens. MRS Online Proceedings Library 209, 289–292 (1990). https://doi.org/10.1557/PROC-209-289
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