Skip to main content
Log in

Investigation of defects and nanoparticles with martensitic phase transformation in surface nanostructured 316L stainless steel by slow-positron beam

  • Article
  • Published:
Journal of Materials Research Aims and scope Submit manuscript

Abstract

In this article, we investigated the defects introduced by surface mechanical attrition treatment by Doppler-broadening spectroscopy of positron annihilation radiation in surface-nanostructured 316L stainless steel. Through the measurement of different thinning layers in the samples treated for 15 min, the slope of line shape parameter S versus wing parameter W curves showed three different values with depth responding to the change of defect configuration. An unusual change of S and W parameters near the surface was mainly from the effect of quantum-dot-like state caused by the formation of nanoparticles. Based on the change of S ˜ W with depth, the martensite phase transformation induced by strain could be estimated to occur within a depth of 35 µm.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. W.P. Tong, N.R. Tao, Z.B. Wang, J. Lu, K. Lu Nitriding iron at lower temperatures. Science 299, 686 (2003)

    Article  CAS  Google Scholar 

  2. TriftshäW. user, KöG. gel Defect structures below the surface in metals investigated by monoenergetic positrons. Phys. Rev. Lett. 48, 1741 (1982)

    Article  Google Scholar 

  3. A. Aruga, S. Takamura, M. Hirose, Y. Itoh Depth profiles of defects in C-ion-irradiated steel determined by a least-squares fit of S parameters from variable-energy positron annihilation. Phys. Rev. B: Condens. Matter 46, 14411 (1992)

    Article  CAS  Google Scholar 

  4. B.J. Kooi, van A. Veen, De J. HossonTh.M. Rectangular nanovoids in helium-implanted and thermally annealed MgO(100). Appl. Phys. Lett. 76, (9) 1110 (2000)

    Article  CAS  Google Scholar 

  5. X. Wang, J. Wang, L. Xiong, G. Liu Defect characteristics in the surface nanocrystallined material treated by high-energy shot peening. Mater. Sci. Forum 445–446, 210 (2004)

    Article  Google Scholar 

  6. K. Lu, J. Lu Nanostructured surface layer on metallic materials induced by surface mechanical attrition treatment. Mater. Sci. Eng., A 375–377, 38 (2004)

    Article  Google Scholar 

  7. R.S. Yu, L. Wei, B.Y. Wang, Z.S. Yin An energy filter for slow positron beam using cosine coils. Nucl. Instrum. Methods Phys. Res., Sect. A 457, 419 (2001)

    Article  CAS  Google Scholar 

  8. A.V. Veen, H. Schut, de J. Vries, R.A. Hakvoort, M.R. Ijpma Analysis of positron profiling data by means of “VEPFIT”. AIP Conf. Proc. 218, 171 (1990)

    Article  Google Scholar 

  9. A.V. Veen, H. Schut, M. Clement, J.M.M. Nijs, A. Kruseman, M.R. Ijpma VEPFIT applied to depth profiling problems. Appl. Surf. Sci. 85, 216 (1995)

    Article  Google Scholar 

  10. A. Dupasquier, G. Ottaviani Defects profiling by positron beams and other technique Positron Spectroscopy of Solids (IOS Press 1995) 581–657

    Google Scholar 

  11. A.V. Veen, A.C. Kruseman, H. Schut, P.E. Mijnarends, B.J. Kooi, J. DeHossonTh.M. Positron analysis of defects in metals. Mater. Sci. Forum 255–257, 76 (1997)

    Article  Google Scholar 

  12. Z. Ni, X. Wang, E. Wu, G. Liu Martensitic phase transformations in the nanostructured surface layers induced by mechanical attrition treatment. J. Appl. Phys. 98, 114319 (2005)

    Article  Google Scholar 

  13. Y. Nagi, M. Hassegawa, Z. Tang, A. Hempel, K. Yubuta, T. Shimamura, Y. Kawazoe, A. Kawai, F. Kano Positron confinement in ultrafine embedded particles: Quantum-dot-like state in an Fe-Cu alloy. Phys. Rev. B: Condens. Matter 61, 6574 (2000)

    Article  Google Scholar 

  14. Y. Nagai, Z. Tang, M. Hasegawa, T. Kanai, M. Saneyasu Irradiation-induced Cu aggregations in Fe: An origin of embrittlement of reactor pressure-vessel steels. Phys. Rev. B: Condens. Matter 63, 134110 (2001)

    Article  Google Scholar 

  15. Y. Nagai, T. Chiba, Z. Tang, T. Akahane, T. Kanai, M. Hasegawa, M. Takenaka, E. Kuramoto Fermi surface of nanocrystalline embedded particles in materials: Bcc Cu in Fe. Phys. Rev. Lett. 87, 176402 (2001)

    Article  CAS  Google Scholar 

  16. T. Onitsuka, M. Takenaka, E. Kuramoto, Y. Nagai, M. Hasegawa Deformation-enhanced Cu precipitation in Fe-Cu alloy studied by positron annihilation spectroscopy. Phys. Rev. B: Condens. Matter 65, 012204 (2001)

    Article  Google Scholar 

  17. M.J. Puska, P. Lanke, R.M. Nieminen Positron affinities for elemental metals. J. Phys. Condens. Matter 1, 6081 (1989)

    Article  CAS  Google Scholar 

  18. R.M. Nieminen Electronic structure and positron spectroscopy of solids and surfaces Positron Spectroscopy of Solids (IOS Press 1995) 443–489

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Xiaowei Wang.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Wang, X., Xiong, L., Liu, X. et al. Investigation of defects and nanoparticles with martensitic phase transformation in surface nanostructured 316L stainless steel by slow-positron beam. Journal of Materials Research 25, 587–591 (2010). https://doi.org/10.1557/JMR.2010.0074

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/JMR.2010.0074

Navigation