Skip to main content
Log in

Nondestructive measurement of striation defect spacing using laser diffraction

  • Articles
  • Published:
Journal of Materials Research Aims and scope Submit manuscript

Abstract

A simple method is presented for measuring the characteristic spacing between striation defects that sometimes develop when coatings are deposited by the spin-coating process. Striation defects, because of their substantial regularity of thickness variation, are able to diffract laser light. By measuring the diffraction angle, it is possible to determine a characteristic spacing that corresponds to the most dominant spatial frequency for the striation defects that have formed. This diffraction technique is compared with other methods for determining the average striation spacing. This noncontact characterization technique may also be applicable to other regularly or quasi-regularly spaced defect structures that appear in coatings or other materials. The limits and accuracy of this technique are discussed in detail.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. D.J. Elliot. and M.A. Hockey, Solid State Technol. 22, 53 (1979).

    Article  CAS  Google Scholar 

  2. B.K. Daniels, C.R. Szmanda, M.K. Templeton, and P. Trefonas, Proc. SPIE. 631, 192 (1986).

    Google Scholar 

  3. R.G. Larson. and T.J. Rehg, in Liquid Film Coating, edited by S.F. Kistler . and P.M. Schweizer . (Chapman & Hall, London, United Kingdom, 1997), pp. 703–734.

    Article  CAS  Google Scholar 

  4. D.E. Haas. and D.P. Birnie. III, (unpublished).

    Google Scholar 

  5. D.E. Haas, D.P. Birnie. III, M.J. Zecchino, and J.T. Figueroa, (unpublished).

  6. D.E. Haas, J.N. Quijada, S.J. Picone, and D.P. Birnie. III, in Sol-Gel Optics V, edited by B.S. Dunn, E.J.A. Pope, H.K. Schmidt, and M. Yamane (Proc. SPIE, Bellingham, WA, 3943, 2000), pp. 280–284.

  7. D.E. Haas. and D.P. Birnie. III, in Proc. Am. Ceram. Soc. Symposium on Sol-Gel Processing, Commercialization & Applications (Ceramic Transactions), edited by Xiangdong Feng, Lisa C. Klein, Edward J.A. Pope, and Sridhar Komarneni (Am. Ceram. Soc., Westerville, OH, 2001), Vol. 123.

    Book  Google Scholar 

  8. D. Leers, Solid State Technology 24, 90 (1981).

    Google Scholar 

  9. P. Frasch and K.H. Saremski, IBM J. Res. Dev. 26, 561 (1982).

    CAS  Google Scholar 

  10. M. Ananst, A. Jamting, J.M. Bell, and B. Ben-Nissan, Thin Solid Films 253, 303 (1994).

    Article  Google Scholar 

  11. T.J. Rehg. and B.G. Higgins, Phys. Fluids 31, 1360 (1988).

    Article  Google Scholar 

  12. T.J. Rehg. and B.G. Higgins, AIChE J. 38, 489 (1992).

    Article  Google Scholar 

  13. M.J. Block, Nature 178, 650 (1956).

    Article  CAS  Google Scholar 

  14. J.R.A. Pearson, J. Fluid Mech. 4, 489 (1958).

    Article  CAS  Google Scholar 

  15. D.A. Nield, J. Fluid Mech. 19, 341 (1964).

    Article  Google Scholar 

  16. E.C. Cobb. and O.A. Saunders, Proc. R. Soc. (London) 236, 343 (1956).

    Article  Google Scholar 

  17. F. Kreith, J.H. Taylor, and J.P. Chong, J. Heat Transfer May, 95 (1959).

    CAS  Google Scholar 

  18. D.P. Birnie. III and M. Manley, Phys. Fluids 9, 870 (1997).

    Google Scholar 

  19. F.A. Jenkins. and H.E. White, Fundamentals of Optics (McGraw-Hill, New York, 1976) p. 360.

    Article  CAS  Google Scholar 

  20. D. Meyerhofer, J. Appl. Phys. 49, 3993 (1978).

    Google Scholar 

  21. A.P. Alivisatos, Science 271, 933 (1996).

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Dunbar P. Birnie III.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Haas, D.E., Birnie, D.P. Nondestructive measurement of striation defect spacing using laser diffraction. Journal of Materials Research 16, 3355–3360 (2001). https://doi.org/10.1557/JMR.2001.0463

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/JMR.2001.0463

Navigation