Abstract
Cross sections through nanoindents on Si, Ge, and GaAs {001} were examined through transmission electron microscopy. A focused ion beam workstation was used to machine electron transparent windows through the indents. In both Si and Ge there was a transformed zone immediately under the indent composed of amorphous material and a mixture of face-centered-cubic and body-centered cubic crystals. Cracking and dislocation generation were also observed around the transformed zone. In GaAs the dominant deformation mechanism was twinning on the {11} planes. The hardness of these materials is discussed in light of these observations and their macroscopic material properties such as phase transformation pressure.
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Lloyd, S.J., Molina-Aldareguia, J.M. & Clegg, W.J. Deformation under nanoindents in Si, Ge, and GaAs examined through transmission electron microscopy. Journal of Materials Research 16, 3347–3350 (2001). https://doi.org/10.1557/JMR.2001.0461
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DOI: https://doi.org/10.1557/JMR.2001.0461